Cited by 259Electrocatalysts for Energy ConversionElectrochemical sensors and biosensorsCatalytic Processes in Materials Science

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Single‐Crystalline Ultrathin Nickel Nanosheets Array from In Situ Topotactic Reduction for Active and Stable Electrocatalysis

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Kuang, Yun, Feng, Guang, Li, Pengsong, Bi, Yongmin, Li, Yaping, Sun, Xiaoming·2016·Angewandte Chemie International Edition

DOI 10.1002/anie.201509616PMC PMC4706644

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Abstract

Simultaneously synthesizing and structuring atomically thick or ultrathin 2D non-precious metal nanocrystal may offer a new class of materials to replace the state-of-art noble-metal electrocatalysts; however, the synthetic strategy is the bottleneck which should be urgently solved. Here we report the synthesis of an ultrathin nickel nanosheet array (Ni-NSA) through in situ topotactic reduction from Ni(OH)2 array precursors. The Ni nanosheets showed a single-crystalline lamellar structure with only ten atomic layers in thickness and an exposed (111) facet. Combined with a superaerophobic (low bubble adhesive) arrayed structure the Ni-NSAs exhibited a dramatic enhancement on both activity and stability towards the hydrazine-oxidation reaction (HzOR) relative to platinum. Furthermore, the partial oxidization of Ni-NSAs in ambient atmosphere resulted in effective water-splitting electrocatalysts for the hydrogen-evolution reaction (HER).

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Authors: Kuang, Y., Feng, G., Li, P., Bi, Y., Li, Y., & Sun, X.
Affiliations: State Key Laboratory of Chemical Resource Engineering (CN)
Corresponding author: Sun, Xiaoming
ORCID: Kuang, Yun
Feng, Guang
Li, Pengsong
Li, Yaping
Sun, Xiaoming
Venue: Angewandte Chemie International Edition
Publisher: Wiley
Published: 2015-11-19
Volume: 55
Issue: 2
Pages: 693-697
ISSN: 1433-7851 (ISSN-L)
1521-3773
DOI: 10.1002/anie.201509616
PMC: PMC4706644
OpenAlex: W2173150847
Cited by: 259
References: 41
Citations by year: 2026: 4 · 2025: 15 · 2024: 13 · 2023: 19 · 2022: 20 · 2021: 39 · 2020: 32 · 2019: 30 · 2018: 32 · 2017: 35 · 2016: 20
FWCI: 8.59
Type: journal article
Language: en
Open access: hybrid
doi.org
Licence: other-oa
onlinelibrary.wiley.com/termsAndConditions#vor (vor)
Locations: Angewandte Chemie International Edition (publishedVersion, other-oa)
PubMed Central (publishedVersion, cc-by-nc)
PubMed (publishedVersion)
Funders: Funded Access
National Natural Science Foundation of China
973 Program (2011CBA00503, 2011CB932403)
Program for Changjiang Scholars and Innovative Research Team in the University
Topics: Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › Electrocatalysts for Energy Conversion
Physical Sciences › Chemistry › Analytical Chemistry › Electrochemical sensors and biosensors
Physical Sciences › Materials Science › Materials Chemistry › Catalytic Processes in Materials Science
Keywords: topotactic reduction, superaerophobic surfaces, hydrazine oxidation, hydrogen evolution reaction, water splitting, non-precious metal electrocatalysts, catalyst stability

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Single‐Crystalline Ultrathin Nickel Nanosheets Array from In Situ Topotactic Reduction for Active and Stable Electrocatalysis

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