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The Common Intermediates of Oxygen Evolution and Dissolution Reactions during Water Electrolysis on Iridium
Open accessAbstract
Understanding the pathways of catalyst degradation during the oxygen evolution reaction is a cornerstone in the development of efficient and stable electrolyzers, since even for the most promising Ir based anodes the harsh reaction conditions are detrimental. The dissolution mechanism is complex and the correlation to the oxygen evolution reaction itself is still poorly understood. Here, by coupling a scanning flow cell with inductively coupled plasma and online electrochemical mass spectrometers, we monitor the oxygen evolution and degradation products of Ir and Ir oxides in situ. It is shown that at high anodic potentials several dissolution routes become possible, including formation of gaseous IrO 3. On the basis of experimental data, possible pathways are proposed for the oxygen‐evolution‐triggered dissolution of Ir and the role of common intermediates for these reactions is discussed.
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Cites
Combining theory and experiment in electrocatalysis: Insights into materials design
Seh, Z. W., Kibsgaard, J., Dickens, C. F., Chorkendorff, I., Nørskov, J. K., & Jaramillo, T. F. (2017) · Science · doi:10.1126/science.aad4998 · Cited by 12,114
Reier, T., Nong, H. N., Teschner, D., Schlögl, R., & Strasser, P. (2017) · Advanced Energy Materials · doi:10.1002/aenm.201601275 · Cited by 1,253
Cited by
Chen, F.-Y., Wu, Z.-Y., Adler, Z., & Wang, H. (2021) · Joule · doi:10.1016/j.joule.2021.05.005 · Cited by 1,284
Bifunctional Electrocatalysts for Overall and Hybrid Water Splitting
Quan, L., Jiang, H., Mei, G., Sun, Y., & You, B. (2024) · Chemical Reviews · doi:10.1021/acs.chemrev.3c00332 · Cited by 874
Ouyang, T., Ye, Y., Wu, C., Xiao, K., & Liu, Z. (2019) · Angewandte Chemie International Edition · doi:10.1002/anie.201814262 · Cited by 804
Fe-Based Electrocatalysts for Oxygen Evolution Reaction: Progress and Perspectives
Feng, C., Faheem, M. B., Fu, J., Xiao, Y., Li, C., & Li, Y. (2020) · ACS Catalysis · doi:10.1021/acscatal.9b05445 · Cited by 587
High-entropy alloys in electrocatalysis: from fundamentals to applications
Ren, J.-T., Chen, L., Wang, H.-Y., & Yuan, Z.-Y. (2023) · Chemical Society Reviews · doi:10.1039/d3cs00557g · Cited by 551
Metadata
- Authors
- Kasian, O., Grote, J., Geiger, S., Cherevko, S., & Mayrhofer, K. J. J.
- Venue
- Angewandte Chemie International Edition
- Publisher
- Wiley
- Published
- 2018-02-05
- Volume
- 57
- Issue
- 9
- Pages
- 2488-2491
- ISSN
- 1433-7851 (ISSN-L)
- 1521-3773
- OpenAlex
- W2773276663
- Cited by
- 559
- References
- 2
- FWCI
- 8.47
- Type
- journal article
- Language
- en
- Open access
- hybrid
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- Kasian, O., Grote, J., Geiger, S., Cherevko, S., & Mayrhofer, K. J. J. (2018). The Common Intermediates of Oxygen Evolution and Dissolution Reactions during Water Electrolysis on Iridium. Angewandte Chemie International Edition. https://doi.org/10.1002/anie.201709652
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