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Adsorbed Intermediates in Oxygen Reduction on Platinum Nanoparticles Observed by In Situ IR Spectroscopy
Open accessAbstract
The sluggish kinetics of oxygen reduction to water remains a significant limitation in the viability of proton‐exchange‐membrane fuel cells, yet details of the four‐electron oxygen reduction reaction remain elusive. Herein, we apply in situ infrared spectroscopy to probe the surface chemistry of a commercial carbon‐supported Pt nanoparticle catalyst during oxygen reduction. The IR spectra show potential‐dependent appearance of adsorbed superoxide and hydroperoxide intermediates on Pt. This strongly supports an associative pathway for oxygen reduction. Analysis of the adsorbates alongside the catalytic current suggests that another pathway must also be in operation, consistent with a parallel dissociative pathway.
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Cites
Origin of the Overpotential for Oxygen Reduction at a Fuel-Cell Cathode
Nørskov, J. K., Rossmeisl, J., Logadottir, A., Lindqvist, L., Kitchin, J. R., Bligaard, T., & Jónsson, H. (2004) · The Journal of Physical Chemistry B · doi:10.1021/jp047349j · Cited by 13,153
Recent Advances in Electrocatalysts for Oxygen Reduction Reaction
Shao, M., Chang, Q., Dodelet, J.-P., & Chenitz, R. (2016) · Chemical Reviews · doi:10.1021/acs.chemrev.5b00462 · Cited by 3,903
Alloys of platinum and early transition metals as oxygen reduction electrocatalysts
Greeley, J., Stephens, I. E. L., Bondarenko, A. S., Johansson, T. P., Hansen, H. A., Jaramillo, T. F., Rossmeisl, J., Chorkendorff, I., & Nørskov, J. K. (2009) · Nature Chemistry · doi:10.1038/nchem.367 · Cited by 3,203
Recent advancements in Pt and Pt-free catalysts for oxygen reduction reaction
Nie, Y., Li, L., & Wei, Z. (2015) · Chemical Society Reviews · doi:10.1039/c4cs00484a · Cited by 2,156
Platinum-Based Oxygen Reduction Electrocatalysts
Wu, J., & Yang, H. (2013) · Accounts of Chemical Research · doi:10.1021/ar300359w · Cited by 1,050
Markovic, N. M., Gasteiger, H. A., & Ross, P. N. (1995) · The Journal of Physical Chemistry · doi:10.1021/j100011a001 · Cited by 736
Cited by
Zhao, Y., Adiyeri Saseendran, D. P., Huang, C., Triana, C. A., Marks, W. R., Chen, H., Zhao, H., & Patzke, G. R. (2023) · Chemical Reviews · doi:10.1021/acs.chemrev.2c00515 · Cited by 802
Chen, S., Luo, T., Li, X., Chen, K., Fu, J., Liu, K., Cai, C., Wang, Q., Li, H., Chen, Y., et al. (2022) · Journal of the American Chemical Society · doi:10.1021/jacs.2c01194 · Cited by 560
Dynamic rhenium dopant boosts ruthenium oxide for durable oxygen evolution
Jin, H., Liu, X., An, P., Tang, C., Yu, H., Zhang, Q., Peng, H.-J., Gu, L., Zheng, Y., Song, T., et al. (2023) · Nature Communications · doi:10.1038/s41467-023-35913-6 · Cited by 409
Review of Carbon Support Coordination Environments for Single Metal Atom Electrocatalysts (SACS)
Song, W., Xiao, C., Ding, J., Huang, Z., Yang, X., Zhang, T., Mitlin, D., & Hu, W. (2024) · Advanced Materials · doi:10.1002/adma.202301477 · Cited by 373
Li, Q., Jiao, Y., Tang, Y., Zhou, J., Wu, B., Jiang, B., & Fu, H. (2023) · Journal of the American Chemical Society · doi:10.1021/jacs.3c05234 · Cited by 339
Metadata
- Authors
- Nayak, S., McPherson, I. J., & Vincent, K. A.
- Venue
- Angewandte Chemie International Edition
- Publisher
- Wiley
- Published
- 2018-08-28
- Volume
- 57
- Issue
- 39
- Pages
- 12855-12858
- ISSN
- 1433-7851 (ISSN-L)
- 1521-3773
- OpenAlex
- W2854976895
- Cited by
- 278
- References
- 6
- FWCI
- 1.64
- Type
- journal article
- Language
- en
- Open access
- green
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- Nayak, S., McPherson, I. J., & Vincent, K. A. (2018). Adsorbed Intermediates in Oxygen Reduction on Platinum Nanoparticles Observed by In Situ IR Spectroscopy. Angewandte Chemie International Edition. https://doi.org/10.1002/anie.201804978
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