Temperature-controlled liquid-liquid microextraction combined with high-performance liquid chromatography for the simultaneous determination of diazinon and fenitrothion in water and fruit juice samples

Bazmandegan‐Shamili, Alireza; Dadfarnia, Shayessteh; Shabani, Ali Mohammad Haji; Moghadam, Masoud Rohani; Saeidi, Mahboubeh

doi:10.1002/jssc.201701427

Cited by 26Analytical chemistry methods developmentPesticide Residue Analysis and SafetyIonic liquids properties and applications

Temperature-controlled liquid-liquid microextraction combined with high-performance liquid chromatography for the simultaneous determination of diazinon and fenitrothion in water and fruit juice samples

Bazmandegan‐Shamili, Alireza, Dadfarnia, Shayessteh, Shabani, Ali Mohammad Haji, Moghadam, Masoud Rohani, Saeidi, Mahboubeh·2018·Journal of Separation Science

DOI 10.1002/jssc.201701427

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Abstract

A simple, environmentally benign, and rapid method based on temperature‐controlled liquid–liquid microextraction using a deep eutectic solvent was developed for the simultaneous extraction/preconcentration of diazinon and fenitrothion. The method involved the addition of deep eutectic solvent to the aqueous sample followed by heating the mixture in a 75°C water bath until the solvent was completely dissolved in the aqueous phase. Then, the resultant solution was cooled in an ice bath and a cloudy solution was formed. Afterward, the mixture was centrifuged and the enriched deep eutectic solvent phase was analyzed by high‐performance liquid chromatography with ultraviolet detection for quantification of the analytes. The factors affecting the extraction efficiency were optimized. Under the optimized extraction conditions, the limits of detection for diazinon and fenitrothion were 0.3 and 0.15 μg/L, respectively. The calibration curves for diazinon and fenitrothion exhibited linearity in the concentration range of 1–100 and 0.5–100 μg/L, respectively. The relative standard deviations for five replicate measurements at 10.0 μg/L level of analytes were less than 2.8 and 4.5% for intra‐ and interday assays, respectively. The developed method was successfully applied to the determination of diazinon and fenitrothion in water and fruit juice samples.

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Authors: Bazmandegan‐Shamili, A., Dadfarnia, S., Shabani, A. M. H., Moghadam, M. R., & Saeidi, M.
Affiliations: Yazd University (IR)
Vali Asr University of Rafsanjan (IR)
Corresponding author: Dadfarnia, Shayessteh
Shabani, Ali Mohammad Haji
ORCID: Bazmandegan‐Shamili, Alireza
Dadfarnia, Shayessteh
Shabani, Ali Mohammad Haji
Moghadam, Masoud Rohani
Venue: Journal of Separation Science
Publisher: Wiley
Published: 2018-04-03
Volume: 41
Issue: 11
Pages: 2411-2418
ISSN: 1615-9306 (ISSN-L)
1615-9314
DOI: 10.1002/jssc.201701427
OpenAlex: W2792307830
Cited by: 25
References: 32
Citations by year: 2026: 1 · 2024: 1 · 2023: 3 · 2022: 3 · 2021: 5 · 2020: 5 · 2019: 6 · 2018: 1
FWCI: 2.65
Type: journal article
Language: en
Open access: closed
Licence: onlinelibrary.wiley.com/termsAndConditions#vor (vor)
Locations: Journal of Separation Science (publishedVersion)
PubMed (publishedVersion)
Topics: Physical Sciences › Chemistry › Analytical Chemistry › Analytical chemistry methods development
Life Sciences › Agricultural and Biological Sciences › Food Science › Pesticide Residue Analysis and Safety
Physical Sciences › Chemical Engineering › Catalysis › Ionic liquids properties and applications
Keywords: diazinon, fenitrothion, organophosphorus pesticides, deep eutectic solvents, preconcentration, simultaneous determination, water analysis, fruit juice analysis, pesticide residues
MeSH terms: Fruit and Vegetable Juices, Chromatography, High Pressure Liquid, Diazinon, Fenitrothion, Food Contamination, Fresh Water, Insecticides, Limit of Detection, Liquid Phase Microextraction

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Temperature-controlled liquid-liquid microextraction combined with high-performance liquid chromatography for the simultaneous determination of diazinon and fenitrothion in water and fruit juice samples

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