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Homogeneous Tritylation of Cellulose in 1‐Butyl‐3‐methylimidazolium Chloride
Abstract
1‐Alkyl‐3‐methylimidazolium‐based ionic liquids, having chloride as a counter ion, were studied for cellulose solubility; and the influence of different alkyl chain lengths was also investigated. The alkyl chain length was incrementally varied from ethyl to decyl to determine structure‐dissolution properties; a distinct odd‐even effect was observed for short chain lengths. In addition, the tritylation of cellulose was performed in 1‐butyl‐3‐methylimidazolium chloride using pyridine as base. The influences of reaction time and the ratio of trityl chloride per cellulose monomer unit on the degree of substitution were investigated in detail by elemental analysis and 1 H NMR spectroscopy. A DS of around 1 was obtained after 3 h reaction time using a six fold excess of trityl chloride. magnified image
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Cites
Dissolution of cellulose with ionic liquids and its application: a mini-review
Zhu, S., Wu, Y., Chen, Q., Yu, Z., Wang, C., Jin, S., Ding, Y., & Wu, G. (2006) · Green Chemistry · doi:10.1039/b601395c · Cited by 1,260
Abbott, A. P., Capper, G., Davies, D. L., Munro, H. L., Rasheed, R. K., & Tambyrajah, V. (2001) · Chemical Communications · doi:10.1039/b106357j · Cited by 1,100
Cited by
Ionic Liquids and Their Interaction with Cellulose
Pinkert, A., Marsh, K. N., Pang, S., & Staiger, M. P. (2009) · Chemical Reviews · doi:10.1021/cr9001947 · Cited by 1,508
Ionic liquid processing of cellulose
Wang, H., Gurau, G., & Rogers, R. D. (2012) · Chemical Society Reviews · doi:10.1039/c2cs15311d · Cited by 1,369
Extended dissolution studies of cellulose in imidazolium based ionic liquids
Vitz, J., Erdmenger, T., Haensch, C., & Schubert, U. S. (2009) · Green Chemistry · doi:10.1039/b818061j · Cited by 462
Self-citationRoom temperature ionic liquids as emerging solvents for the pretreatment of lignocellulosic biomass
Mora‐Pale, M., Meli, L., Doherty, T. V., Linhardt, R. J., & Dordick, J. S. (2011) · Biotechnology and Bioengineering · doi:10.1002/bit.23108 · Cited by 384
Cellulose Solvents – Remarkable History, Bright Future
Liebert, T. (2010) · ACS Symposium Series · doi:10.1021/bk-2010-1033.ch001 · Cited by 250
Metadata
- Authors
- Erdmenger, T., Haensch, C., Hoogenboom, R., & Schubert, U. S.
- Venue
- Macromolecular Bioscience
- Publisher
- Wiley
- Published
- 2007-04-10
- Volume
- 7
- Issue
- 4
- Pages
- 440-445
- ISSN
- 1616-5187 (ISSN-L)
- 1616-5195
- OpenAlex
- W2073353689
- Cited by
- 182
- References
- 2
- FWCI
- 4.98
- Type
- journal article
- Language
- en
- Open access
- closed
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- Erdmenger, T., Haensch, C., Hoogenboom, R., & Schubert, U. S. (2007). Homogeneous Tritylation of Cellulose in 1‐Butyl‐3‐methylimidazolium Chloride. Macromolecular Bioscience. https://doi.org/10.1002/mabi.200600253
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