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Determination of the structure of active centers in the anionic polymerization by 31 P NMR, introducing a P‐containing end group
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An additional possibility for determining whether route alpha or beta is preferred is to short stop the polymerization with diphenyl chlorophosphate and analyze the solution with 31P NMR.
“An additional possibility for determining whether route α or β (Figure 40) is preferred is to short stop the polymerization e.g., with diphenyl chlorophosphate (see Figure 41) and then to analyze the solution with 31 P NMR [114,115].”
From Ring-Opening Polymerization—An Introductory Review (2013) · cites this paper as [114]
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Metadata
- Authors
- Sosnowski, S., Duda, A., Słomkowski, S., & Penczek, S.
- Affiliations
- Centrum Badań Molekularnych i Makromolekularnych Polskiej Akademii Nauk (PL)
- Corresponding author
- Penczek, Stanisław
- Venue
- Die Makromolekulare Chemie, Rapid Communications
- Publisher
- Wiley
- Published
- 1984-09
- Volume
- 5
- Issue
- 9
- Pages
- 551-557
- ISSN
- 0173-2803 (ISSN-L)
- OpenAlex
- W1529815068
- Cited by
- 45
- References
- 15
- Citations by year
- 2026: 1 · 2022: 1 · 2021: 1 · 2020: 1 · 2017: 1 · 2016: 2 · 2013: 2 · 2012: 1
- FWCI
- 2.79
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- Die Makromolekulare Chemie Rapid Communications (publishedVersion)
- Topics
- Physical Sciences › Chemistry › Organic Chemistry › Advanced Polymer Synthesis and Characterization
- Physical Sciences › Chemistry › Organic Chemistry › Organometallic Complex Synthesis and Catalysis
- Physical Sciences › Materials Science › Polymers and Plastics › Polymer Synthesis and Characterization
- Keywords
- anionic polymerization, active centers, 31P NMR, polymer end groups, polymer structure determination
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