The DOI matches its Crossref record; 22 of the 22 references it cites were found in a registry or an index.
Gas chromatography‐mass spectrometry methods for structural analysis of fatty acids
Abstract
Procedures for structural analysis of fatty acids are reviewed. The emphasis is on methods that involve gas chromatography‐mass spectrometry and, in particular, the use of picolinyl ester and dimethyloxazoline derivatives. These should be considered as complementing each other, not simply as alternatives. However, additional derivatization procedures can be of value, including hydrogenation and deuteration, and preparation of dimethyl disulfide and 4‐methyl‐1,2,4‐triazoline‐3,5‐dione adducts. Sometimes complex mixtures must be separated into simpler fractions prior to analysis by gas chromatography‐mass spectrometry. Silver ion and reversed‐phase high‐performance liquid chromatography are then of special value. In particular, a novel application of the latter technique, involving a base‐deactivated stationary phase and acetonitrile as mobile phase, is described that is suited to the separation of fatty acids in the form of picolinyl ester and dimethyloxazoline derivatives, as well as methyl esters.
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Cites
Christie, W. W. (1989) · Medical Entomology and Zoology · Cited by 1,044
Self-citationChristie, W. W. (1989) · Cited by 486
Self-citationStructure and occurrence of unusual fatty acids in minor seed oils
BADAMI, R., & PATIL, K. (1980) · Progress in Lipid Research · doi:10.1016/0163-7827(80)90002-8 · Cited by 321
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Advances in Lipid Methodology — One
Murphy, E. J. (1994) · Chemistry and Physics of Lipids · doi:10.1016/0009-3084(94)90040-x · Cited by 228
Gas chromatography and lipids a practical guide
Egge, H. (1990) · Chemistry and Physics of Lipids · doi:10.1016/0009-3084(90)90141-d · Cited by 226
Silver ion chromatography of lipids and fatty acids
Dobson, G., Christie, W. W., & Nikolova-Damyanova, B. (1995) · Journal of Chromatography B: Biomedical Sciences and Applications · doi:10.1016/0378-4347(95)00157-e · Cited by 208
Self-citationHarvey, D. J. (1982) · Biological Mass Spectrometry · doi:10.1002/bms.1200090107 · Cited by 201
Metabolites of conjugated isomers of linoleic acid (CLA) in the rat
Sébédio, J. L., Juanéda, P., Dobson, G., Ramilison, I., Martin, J. C., Chardigny, J. M., & Christie, W. W. (1997) · Biochimica et Biophysica Acta (BBA) - Lipids and Lipid Metabolism · doi:10.1016/s0005-2760(97)00015-5 · Cited by 183
Self-citationZhang, J. Y., Yu, Q. T., Liu, B. N., & Huang, Z. H. (1988) · Biological Mass Spectrometry · doi:10.1002/bms.1200150106 · Cited by 167
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Integrated CO2 capture, wastewater treatment and biofuel production by microalgae culturing—A review
Razzak, S. A., Hossain, M. M., Lucky, R. A., Bassi, A. S., & de Lasa, H. (2013) · Renewable and Sustainable Energy Reviews · doi:10.1016/j.rser.2013.05.063 · Cited by 631
Advances in Chemical and Biological Methods to Identify Microorganisms—From Past to Present
Franco-Duarte, R., Černáková, L., Kadam, S., S. Kaushik, K., Salehi, B., Bevilacqua, A., Corbo, M. R., Antolak, H., Dybka-Stępień, K., Leszczewicz, M., et al. (2019) · Microorganisms · doi:10.3390/microorganisms7050130 · Cited by 565
A vertebrate fatty acid desaturase with Δ5 and Δ6 activities
Hastings, N., Agaba, M., Tocher, D. R., Leaver, M. J., Dick, J. R., Sargent, J. R., & Teale, A. J. (2001) · Proceedings of the National Academy of Sciences · doi:10.1073/pnas.251516598 · Cited by 345
Analytical strategies for identifying drug metabolites
Prakash, C., Shaffer, C. L., & Nedderman, A. (2007) · Mass Spectrometry Reviews · doi:10.1002/mas.20128 · Cited by 302
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Shingfield, K. J., & Griinari, J. M. (2007) · European Journal of Lipid Science and Technology · doi:10.1002/ejlt.200700026 · Cited by 228
Metadata
- Authors
- Christie, W. W.
- Venue
- Lipids
- Publisher
- Wiley
- Published
- 1998-04
- Volume
- 33
- Issue
- 4
- Pages
- 343-353
- ISSN
- 0024-4201 (ISSN-L)
- 1558-9307
- OpenAlex
- W2054091689
- Cited by
- 347
- References
- 22
- FWCI
- 3.83
- Type
- journal article
- Language
- en
- Open access
- closed
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Bibliographic data: Semantic Scholar, OpenAlex, Crossref.
Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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