The DOI matches its Crossref record; 12 of the 12 references it cites were found in a registry or an index.
Critical temperatures in the synthesis of graphene-like materials by thermal exfoliation–reduction of graphite oxide
Open accessAbstract
Abstract We prepared a series of graphene-like materials by thermal exfoliation/reduction of a graphite oxide (GO) at temperatures between 127 °C and 2400 °C. The extent of the exfoliation and reduction of the GO at different temperatures, as well as the impact on the resultant graphene-like materials (TRGs), were studied through their chemical/structural characterization. The main oxygen loss was observed at 127 °C during the blasting of the GO, which produced its exfoliation into monolayer functionalized TRG with hydroxyl groups and minor amounts of epoxy and carboxyl groups. Above 600 °C, the reduction continued smoothly, with oxygen and hydrogen loss and the conversion of hybridised carbon atoms from sp3 into sp2. 1000 °C appears to be a critical temperature for the efficiency of the reduction process, as the resulting TRG contained
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Cites
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Cited by
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Self-citationEnhanced reduction of graphene oxide by high-pressure hydrothermal treatment
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Graphene oxide synthesis, properties and characterization techniques: a comprehensive review
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N-doped graphene catalysts with high nitrogen concentration for the oxygen reduction reaction
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Metadata
- Authors
- Botas, C., Álvarez, P., Blanco, C., Santamaría, R., Granda, M., Gutiérrez, M. D., Rodríguez-Reinoso, F., & Menéndez, R.
- Venue
- Carbon
- Publisher
- Elsevier BV
- Published
- 2013-02
- Volume
- 52
- Pages
- 476-485
- ISSN
- 0008-6223 (ISSN-L)
- OpenAlex
- W2026457916
- Cited by
- 289
- References
- 12
- FWCI
- 6.52
- Type
- journal article
- Language
- en
- Open access
- green
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