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Cited by 98Gold and Silver Nanoparticles Synthesis and ApplicationsLaser-Ablation Synthesis of NanoparticlesBiosensors and Analytical Detection

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Lignin-mediated green synthesis of functionalized gold nanoparticles via pulsed laser technique for selective colorimetric detection of lead ions in aqueous media

Yu, Yiseul, Naik, Shreyanka Shankar, Oh, Yewon, Theerthagiri, Jayaraman, Lee, Seung Jun, Choi, Myong Yong·2021·Journal of Hazardous Materials
DOI 10.1016/j.jhazmat.2021.126585
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Abstract

A versatile green synthesis technique of pulsed laser irradiation and the sonochemical process was used for the production of functionalized gold nanoparticles (Au NPs) in the presence of lignin matrixes. In this study, the futuristic advantages of the lignin biopolymer were explored for the preparation of zero-valent Au NPs in the absence of any other reducing agents. The resulting lignin functionalized Au NPs (L-Au f NPs) were characterized via high-resolution transmission electron microscopy, X-ray diffraction, UV-vis spectroscopy, and Fourier-transform infrared spectroscopy. The optimum lignin concentration can generate uniformly dispersed crystalline L-Au f NPs. The optimized L-Au f (1-5) NPs permit the selective colorimetric detection of heavy metal ions; thus, the L-Au f (1-5) NPs demonstrated a highly selective colorimetric sensing tendency toward Pb 2+ ions within a short time interval among the various metal ions (Pb 2+, Fe 3+, Cu 2+, Cr 6+, Co 2+, Ag 2+, Ca 2+, Cd 2+, Ba 2+, and Hg 2+). The prominent color change of L-Au f NPs from red wine to purple indicates the detection of Pb 2+ ions. This robust characteristic nature of L-Au f (1-5) NPs can also detect very low concentrations of 1.8 μM in the linear range of 0.1-1 mM. Hence, the outcome of this study coincides with existing studies and indicates that L-Au f (1-5) NPs can also be used as effective sensors for the rapid and selective detection of Pb 2+ ions via the colorimetric analysis using the real environmental samples.

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Metadata

Authors
Yu, Y., Naik, S. S., Oh, Y., Theerthagiri, J., Lee, S. J., & Choi, M. Y.
Affiliations
Gyeongsang National University (KR)
Corresponding author
Choi, Myong Yong
ORCID
Venue
Journal of Hazardous Materials
Publisher
Elsevier BV
Published
2021-10
Volume
420
Pages
126585
ISSN
0304-3894 (ISSN-L)
DOI
10.1016/j.jhazmat.2021.126585
OpenAlex
W3181935066
Cited by
98
References
1
Citations by year
2026: 7 · 2025: 13 · 2024: 13 · 2023: 21 · 2022: 33 · 2021: 11
FWCI
4.75
Type
journal article
Language
en
Open access
closed
Licence
Locations
  • Journal of Hazardous Materials (publishedVersion)
  • PubMed (publishedVersion)
Topics
  • Physical Sciences › Materials Science › Electronic, Optical and Magnetic Materials › Gold and Silver Nanoparticles Synthesis and Applications
  • Physical Sciences › Materials Science › Materials Chemistry › Laser-Ablation Synthesis of Nanoparticles
  • Physical Sciences › Engineering › Biomedical Engineering › Biosensors and Analytical Detection
Keywords
lignin, gold nanoparticles, green synthesis, pulsed laser irradiation, sonochemical synthesis, colorimetric sensing, lead ion detection, heavy metal ions, nanoparticle functionalization, environmental water samples
MeSH terms
Colorimetry, Gold, Ions, Lasers, Lead, Lignin, Metal Nanoparticles

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