Thermal and spectroscopic studies of zeolites exchanged with metal cations

Castaldi, Paola; Santona, Laura; Cozza, Claudio; Giuliano, Veronica; Abbruzzese, Carlo; Nastro, Valentina; Melis, Pietro

doi:10.1016/j.molstruc.2004.09.009

Cited by 105Zeolite Catalysis and SynthesisClay minerals and soil interactionsChemical Synthesis and Characterization

Thermal and spectroscopic studies of zeolites exchanged with metal cations

Castaldi, Paola, Santona, Laura, Cozza, Claudio, Giuliano, Veronica, Abbruzzese, Carlo, Nastro, Valentina, Melis, Pietro·2005·Journal of Molecular Structure

DOI 10.1016/j.molstruc.2004.09.009

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When ion exchange is performed, the water adsorption capacity of clinoptilolite may be modified due to the presence of cations with different charges and/or ionic radii in the framework.
“when ion exchange is performed, the water adsorption capacity of clinoptilolite may be modified due to the presence of cations with different charges and/or ionic radii in the framework (Castaldi et al. 2005).”
From Fundamental properties and sustainable applications of the natural zeolite clinoptilolite (2024) · cites this paper as Castaldi et al. 2005
Between 450 °C and 500 °C, structural water is lost and destruction of the zeolite framework occurs.
“between 450 °C and 500 °C, structural water is lost and then the destruction of zeolite’s framework occurs.”
From Fundamental properties and sustainable applications of the natural zeolite clinoptilolite (2024) · cites this paper as Castaldi et al. 2005
The amount of water lost in the 150-250 °C region is higher for clinoptilolite exchanged with bivalent cations because of greater interaction between these cations and water, resulting in higher thermal stability.
“the amount of water lost in this region turned out to be higher for clinoptilolite exchanged with bivalent cations and this happened because of the grater interaction between these cations and water, which resulted also in higher thermal stability.”
From Fundamental properties and sustainable applications of the natural zeolite clinoptilolite (2024) · cites this paper as Castaldi et al. 2005
Weakly bound water is lost between 60 and 150 °C, whereas water located in cavities and bound to extra-framework cations is lost at 150-250 °C.
“weakly bound water was lost in the range between 60 and 150 °C whereas at 150–250 °C it was possible to observe the loss of water located in the cavities and bound to extra-framework cations.”
From Fundamental properties and sustainable applications of the natural zeolite clinoptilolite (2024) · cites this paper as Castaldi et al. 2005
Thermo-analytical data proved the existence of three dehydration steps, depending on the type of water lost, occurring at three different temperatures.
“the thermo-analytical data proved the existence of three “dehydration steps” (depending on the type of water lost), occurring at three different temperatures.”
From Fundamental properties and sustainable applications of the natural zeolite clinoptilolite (2024) · cites this paper as Castaldi et al. 2005

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Authors: Castaldi, P., Santona, L., Cozza, C., Giuliano, V., Abbruzzese, C., Nastro, V., & Melis, P.
Affiliations: University of Sassari (IT)
Institute of Environmental Geology and Geoengineering (IT)
University of Calabria (IT)
Corresponding author: Melis, Pietro
ORCID: Castaldi, Paola
Venue: Journal of Molecular Structure
Publisher: Elsevier BV
Published: 2005-01
Volume: 734
Issue: 1-3
Pages: 99-105
ISSN: 0022-2860 (ISSN-L)
DOI: 10.1016/j.molstruc.2004.09.009
OpenAlex: W2057869295
Cited by: 104
References: 29
Citations by year: 2026: 2 · 2025: 6 · 2024: 7 · 2023: 2 · 2022: 3 · 2021: 8 · 2020: 6 · 2019: 5 · 2018: 6 · 2017: 3 · 2016: 5 · 2015: 8 · 2014: 7 · 2013: 7 · 2012: 3
FWCI: 1.38
Type: journal article
Language: en
Open access: closed
Licence: www.elsevier.com/tdm/userlicense/1.0/ (tdm)
Locations: Journal of Molecular Structure (publishedVersion)
UnissResearch (Università degli Studi di Sassari) (submittedVersion)
Topics: Physical Sciences › Chemistry › Inorganic Chemistry › Zeolite Catalysis and Synthesis
Physical Sciences › Materials Science › Biomaterials › Clay minerals and soil interactions
Physical Sciences › Environmental Science › Waste Management and Disposal › Chemical Synthesis and Characterization
Keywords: zeolites, cation exchange, metal cations, thermal stability, water desorption, basicity, sodium, potassium, ammonium, lead, cadmium, zinc

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