One minute synthesis of amino-silane functionalized superparamagnetic iron oxide nanoparticles by sonochemical method
Open accessAbstract
Superparamagnetic iron oxide nanoparticles (SPION) are material of interest for biomedical research and related applications. Recently, several works have reported facile sonochemical method of functionalizing nanoparticles with organic coupling agents. Herein, we present the influence of ultrasonic irradiation on the rate of functionalization of 3-amino propyl triethoxyl silane (APTES) on SPION. The effect of sonication on the process is investigated by varying the sonication period between 1 and 20min. Grafting of the organo-metallic molecules on SPION is demonstrated through FTIR and XPS. The results show that in one minute, organo-silane compound can be functionalized onto SPION through unique conditions generated from ultrasonic irradiation. The XPS survey spectra of the as-synthesized APTES-SPION at different sonication periods revealed that absorbed energy due to silanization reactions in all the samples appeared at same peaks. The percentage atomic concentrations of all the elements present in the as-synthesized APTES-SPION are determined by the software CASAXPS. The result demonstrated that highest percentage atomic concentration is observed at the one minute sonication period.
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Amorphous SPION obtained from sonochemical synthesis need further heat-treatment after synthesis.
“Thus, the obtained amorphous SPION need to be further processed by heat-treatment after they have been synthesized [3, 28, 46–48].”
From Iron oxide nanoparticles: Diagnostic, therapeutic and theranostic applications (2019) · cites this paper as [47]
Prototypic examples of materials used to coat iron oxide nanoparticles are polymers, fatty acids, amino acids, metals, and oxides.
“Prototypic examples of materials used to coat iron oxide nanoparticles are polymers [28, 47, 50], fatty acids (like oleic acid, stearic acid, lauric acid and dodecylphosphonic acid) [51–55], amino acids (like phenyl alanine, tyrosine, arginine, lysine and cysteine) [56–58],_metals (like gold, gadolinium and silver) [59–61] and oxides (like silica and TiO2) [62–64].”
From Iron oxide nanoparticles: Diagnostic, therapeutic and theranostic applications (2019) · cites this paper as [47]
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Iron oxide nanoparticles: Diagnostic, therapeutic and theranostic applications
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- Authors
- Sodipo, B. K., & Aziz, A. A.
- Affiliations
- Kaduna State University (NG)
- Universiti Sains Malaysia (MY)
- Corresponding author
- Sodipo, Bashiru K.
- Venue
- Ultrasonics Sonochemistry
- Publisher
- Elsevier BV
- Published
- 2018-01
- Volume
- 40
- Issue
- Pt A
- Pages
- 837-840
- ISSN
- 1350-4177 (ISSN-L)
- OpenAlex
- W2753258508
- Cited by
- 64
- References
- 18
- Citations by year
- 2025: 5 · 2024: 7 · 2023: 8 · 2022: 9 · 2021: 15 · 2020: 7 · 2019: 11 · 2018: 2
- FWCI
- 2.31
- Type
- journal article
- Language
- en
- Open access
- hybrid
- doi.org
- Licence
- Locations
- Ultrasonics Sonochemistry (publishedVersion, cc-by-nc-nd)
- PubMed (publishedVersion)
- Topics
- Physical Sciences › Materials Science › Materials Chemistry › Ultrasound and Cavitation Phenomena
- Physical Sciences › Engineering › Biomedical Engineering › Characterization and Applications of Magnetic Nanoparticles
- Physical Sciences › Materials Science › Materials Chemistry › Magnetic Properties and Synthesis of Ferrites
- Keywords
- superparamagnetic iron oxide nanoparticles, 3-aminopropyltriethoxysilane, silanization, sonication, sonication time, surface functionalization, atomic concentration
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