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Cited by 258

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A new chromatographic system for vitamin D3, and its metabolites: resolution of a new vitamin D3, metabolite

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HOLICK, M.F., DeLUCA, H.F.·1971·Journal of Lipid Research
DOI 10.1016/s0022-2275(20)39495-5
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Abstract

A simple yet powerful new chromatographic procedure for vitamin D(3) and its metabolites is described. Liquid-gel partition chromatography on Sephadex LH-20 using a solvent of various percentages of CHCl(3) in Skellysolve B (petroleum ether, bp 67-69 degrees C) permits excellent resolution of vitamin D(3), 25-hydroxyvitamin D(3), and their more polar metabolites. Of special importance is the resolution of the metabolites of vitamin D(3) more polar than 25-hydroxycholecalciferol. Because of this resolution, a new metabolite of vitamin D(3) has been demonstrated in the plasma of rats and in the intestines of chicks given 100 IU of vitamin D(3)-1,2-(3)H.

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Metadata

Authors
HOLICK, M. F., & DeLUCA, H. F.
Venue
Journal of Lipid Research
Publisher
Elsevier BV
Published
1971-07
Volume
12
Issue
4
Pages
460-465
ISSN
0022-2275 (ISSN-L)
DOI
10.1016/s0022-2275(20)39495-5
OpenAlex
W2152828858
Cited by
258
References
0
FWCI
34.17
Type
journal article
Language
en
Open access
hybrid

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HOLICK, M. F., & DeLUCA, H. F. (1971). A new chromatographic system for vitamin D3, and its metabolites: resolution of a new vitamin D3, metabolite. Journal of Lipid Research. https://doi.org/10.1016/s0022-2275(20)39495-5

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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).

Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.