The DOI matches its Crossref record; 3 of the 3 references it cites were found in a registry or an index.
Large-Scale Synthesis of Monodisperse UiO-66 Crystals with Tunable Sizes and Missing Linker Defects via Acid/Base Co-Modulation
Abstract
Beyond their pore structures and surface chemistry, precise controls over other attributes of metal-organic frameworks (MOFs) such as shapes, sizes, and defects are also favorable to their fundamental studies and applications but still remain challenging. Herein, we reported an acid/base co-modulation strategy to the large-scale synthesis of monodisperse UiO-66 crystals with acetic acid for modulating crystal shape and with triethylamine (TEA) as a base for controlling the nucleation of crystallization and tuning the formation of missing linker defects via promoting presumably the singe deprotonation of terephthalic acid linkers. The obtained monodisperse MOF crystals have a well-defined octahedral shape, tunable sizes ranging from ∼500 nm to ∼2 μm, and high thermal stability. Their assembled-monolayers are responsive to methanol vapor with the crystal size-dependent and defect-relevant sensing performances.
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Cites
Metal-organic framework materials as catalysts
Lee, J., Farha, O. K., Roberts, J., Scheidt, K. A., Nguyen, S. T., & Hupp, J. T. (2009) · Chemical Society Reviews · doi:10.1039/b807080f · Cited by 7,969
Horike, S., Shimomura, S., & Kitagawa, S. (2009) · Nature Chemistry · doi:10.1038/nchem.444 · Cited by 2,486
Metal–organic frameworks as platforms for clean energy
Li, S.-L., & Xu, Q. (2013) · Energy & Environmental Science · doi:10.1039/c3ee40507a · Cited by 970
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Winarta, J., Shan, B., Mcintyre, S. M., Ye, L., Wang, C., Liu, J., & Mu, B. (2020) · Crystal Growth & Design · doi:10.1021/acs.cgd.9b00955 · Cited by 641
Xiang, W., Zhang, Y., Chen, Y., Liu, C.-J., & Tu, X. (2020) · Journal of Materials Chemistry A · doi:10.1039/d0ta08009h · Cited by 359
Nanoscale covalent organic frameworks: from controlled synthesis to cancer therapy
He, X., Jiang, Z., Akakuru, O. U., Li, J., & Wu, A. (2021) · Chemical Communications · doi:10.1039/d1cc04846e · Cited by 303
Metadata
- Authors
- Zhao, Y., Zhang, Q., Li, Y., Zhang, R., & Lu, G.
- Venue
- ACS Applied Materials & Interfaces
- Publisher
- American Chemical Society (ACS)
- Published
- 2017-04-20
- Volume
- 9
- Issue
- 17
- Pages
- 15079-15085
- ISSN
- 1944-8244 (ISSN-L)
- 1944-8252
- OpenAlex
- W2606213681
- Cited by
- 180
- References
- 3
- FWCI
- 5.07
- Type
- journal article
- Language
- en
- Open access
- closed
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