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Asymmetric membrane containing ionic liquid [A336] [P507] for the preconcentration and separation of heavy rare earth lutetium
Abstract
A novel polymer inclusion membrane (PIM) was prepared for the preconcentration and separation of heavy rare earth element (HREE) Lutetium (Lu) from dilute solution. The membrane was composed of poly(vinylidene fluoride) (PVDF) as a matrix and bifunctional ionic liquid extractant [tricaprylmethylammonium][di(2-ethylhexyl)orthophosphinate] ([A336][P507]) as carrier, without any plasticizer. A weak physical effect existed between PVDF chain segment and [A336][P507], but no chemical interaction. Structure characterization and transport experiment both proved the membrane to be an asymmetric structure and LuCl 3 would transport faster from surface with small pores to large pores. YbCl 3 was transported much faster than LuCl 3 which was different in liquid–liquid extraction. Preconcentration experiment realized a great acceleration on the transport of LuCl 3 . And the PIM was proved stable and durable. All these would provide a novel approach to the preconcentration and separation of Lu from dilute solution like leachate of southern ion adsorbed rare earth deposit.
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ILMs have successfully been used for critical and heavy metals from aqueous solutions.
“ILMs have successfully been used for critical and heavy metals from aqueous solutions (Chen and Chen, 2016; Makanyire et al., 2016; Zante et al., 2019; Imdad and Dohare, 2022).”
From A review of technologies for direct lithium extraction from low Li+ concentration aqueous solutions (2022) · cites this paper as Chen and Chen, 2016
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Metadata
- Authors
- Chen, L., & Chen, J.
- Affiliations
- Chinese Academy of Sciences (CN)
- Corresponding author
- Chen, Ji
- Venue
- ACS Sustainable Chemistry & Engineering
- Publisher
- American Chemical Society (ACS)
- Published
- 2016-04-04
- Volume
- 4
- Issue
- 5
- Pages
- 2644-2650
- ISSN
- 2168-0485 (ISSN-L)
- OpenAlex
- W2304316933
- Cited by
- 72
- References
- 29
- Citations by year
- 2026: 5 · 2025: 6 · 2024: 13 · 2023: 6 · 2022: 10 · 2021: 10 · 2020: 5 · 2019: 6 · 2018: 5 · 2017: 5 · 2016: 1
- FWCI
- 5.04
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- ACS Sustainable Chemistry & Engineering (publishedVersion)
- Funders
- Ministry of Science and Technology of the People's Republic of China (2012CBA01202)
- National Natural Science Foundation of China (51174184)
- Chinese Academy of Sciences (KGZD-EW-201-1)
- Topics
- Physical Sciences › Materials Science › Metals and Alloys › Extraction and Separation Processes
- Physical Sciences › Chemistry › Analytical Chemistry › Analytical chemistry methods development
- Physical Sciences › Chemistry › Inorganic Chemistry › Radioactive element chemistry and processing
- Keywords
- polymer inclusion membranes, lutetium, heavy rare earth elements, rare earth separation, preconcentration, asymmetric membranes, polyvinylidene fluoride, ionic liquid extractant, membrane stability, ion transport
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