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Controlled Synthesis of Mesoporous MnO/C Networks by Microwave Irradiation and Their Enhanced Lithium-Storage Properties
Abstract
A rapid and controllable route is developed for the synthesis of MnO nanoparticles that are encapsulated uniformly in three-dimensional (3D) mesoporous interconnected carbon networks (MnO-MICN) through an efficient microwave-polyol process, combined with a subsequent thermal treatment. The dependence of sodium citrate on the morphology of the Mn-based precursors was investigated systematically. Results show that the unique mesoporous interconnected carbon network (MICN) can not only buffer the large volume expansion of MnO during the electrochemical cycling, but also improve the electrode/electrolyte contact area, favoring the fast Li-ion transport and high specific capacity, superior cyclability, and excellent rate capability. When evaluated as an anode material for lithium-ion batteries, the as-formed 3D MnO-MICN nanocomposite exhibits a highly reversible capacity of 1224 mA h g(-1), with a Coulombic efficiency of ~99% at a current density of 200 mA g(-1) over 200 cycles.
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Citations
Cited by
Microwave-Assisted Preparation of Inorganic Nanostructures in Liquid Phase
Zhu, Y.-J., & Chen, F. (2014) · Chemical Reviews · doi:10.1021/cr400366s · Cited by 912
Nanostructured Mo-based electrode materials for electrochemical energy storage
Hu, X., Zhang, W., Liu, X., Mei, Y., & Huang, Y. (2015) · Chemical Society Reviews · doi:10.1039/c4cs00350k · Cited by 711
Self-citationExploring Anomalous Charge Storage in Anode Materials for Next-Generation Li Rechargeable Batteries
Kim, H., Choi, W., Yoon, J., Um, J. H., Lee, W., Kim, J., Cabana, J., & Yoon, W.-S. (2020) · Chemical Reviews · doi:10.1021/acs.chemrev.9b00618 · Cited by 527
Conversion Reaction‐Based Oxide Nanomaterials for Lithium Ion Battery Anodes
Yu, S., Lee, S. H., Lee, D. J., Sung, Y., & Hyeon, T. (2016) · Small · doi:10.1002/smll.201502299 · Cited by 499
Manganese Oxide/Carbon Yolk–Shell Nanorod Anodes for High Capacity Lithium Batteries
Cai, Z., Xu, L., Yan, M., Han, C., He, L., Hercule, K. M., Niu, C., Yuan, Z., Xu, W., Qu, L., et al. (2015) · Nano Letters · doi:10.1021/nl504427d · Cited by 366
Metadata
- Authors
- Luo, W., Hu, X., Sun, Y., & Huang, Y.
- Venue
- ACS Applied Materials & Interfaces
- Publisher
- American Chemical Society (ACS)
- Published
- 2013-03-06
- Volume
- 5
- Issue
- 6
- Pages
- 1997-2003
- ISSN
- 1944-8244 (ISSN-L)
- 1944-8252
- OpenAlex
- W2037031046
- Cited by
- 171
- References
- 0
- FWCI
- 16.58
- Type
- journal article
- Language
- en
- Open access
- closed
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