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Cited by 347

The DOI matches its Crossref record; 26 of the 26 references it cites were found in a registry or an index.

Preparation of Chitin Nanofibers from Squid Pen β-Chitin by Simple Mechanical Treatment under Acid Conditions

Fan, Yimin, Saito, Tsuguyuki, Isogai, Akira·2008·Biomacromolecules

Abstract

A procedure for preparing individualized chitin nanofibers 3-4 nm in cross-sectional width and at least a few microns in length was developed. The key factors to prepare the chitin nanofibers with such high aspect ratios are as follows: (1) squid pen beta-chitin is used as the starting material and (2) ultrasonication of the beta-chitin in water at pH 3-4 and 0.1-0.3% consistency for a few minutes. Transparent and highly viscous dispersions of squid pen beta-chitin nanofibers in water can be obtained by this method. No N-deacetylation occurs on the chitin molecules during the nanofiber conversion procedure. Moreover, the original crystal structure of beta-chitin is maintained, although crystallinity index decreases from 0.51 to 0.37 as a result of the nanofiber conversion. Cationization of the C2 amino groups present on the crystallite surfaces of the squid pen beta-chitin under acid conditions is necessary for preparing the nanofibers.

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Metadata

Authors
Fan, Y., Saito, T., & Isogai, A.
Venue
Biomacromolecules
Published
2008-06-12
Volume
9
Issue
7
Pages
1919-1923
ISSN
  • 1525-7797 (ISSN-L)
  • 1526-4602
OpenAlex
W2048833979
Cited by
347
References
26
FWCI
3.72
Type
journal article
Language
en
Open access
closed

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