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Selective Preparation of Monoclinic and Tetragonal BiVO4with Scheelite Structure and Their Photocatalytic Properties
Abstract
BiVO 4 powder with scheelite structure was obtained by hydrolyzing a nitric acid solution of Bi(NO 3 ) 3 and Na 3 VO 4 with bases (Na 2 CO 3 and NaHCO 3 ) at room temperature. Tetragonal BiVO 4 of a high-temperature form was obtained after 4.5 h of preparation time while monoclinic BiVO 4 was done after 46 h. Although the structure and the band gap of tetragonal BiVO 4 with scheelite structure were similar to those of monoclinic BiVO 4, the photocatalytic activity of the tetragonal BiVO 4 for O 2 evolution from an aqueous AgNO 3 solution under visible light irradiation was negligible. In contrast, the monoclinic BiVO 4 showed high photocatalytic activity. Distortion of a Bi−O polyhedron by a 6s 2 lone pair of Bi 3+ plays an important role for high photocatalytic activity of the monoclinic BiVO 4 under visible light irradiation.
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Metadata
- Authors
- Tokunaga, S., Kato, H., & Kudo, A.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2001-11-30
- Volume
- 13
- Issue
- 12
- Pages
- 4624-4628
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W1995753210
- Cited by
- 1,112
- References
- 0
- FWCI
- 5.15
- Type
- journal article
- Language
- en
- Open access
- closed
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