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Hydrothermal Synthesis of Monodisperse Magnetite Nanoparticles
Abstract
Magnetite particles with an average size of 39 nm and good monodispersity have been synthesized by coprecipitation at 70 °C from ferrous Fe 2+ and ferric Fe 3+ ions by a (N(CH 3 ) 4 OH) solution, followed by hydrothermal treatment at 250 °C. The magnetite nanoparticles before the hydrothermal step display an average size of 12 nm and are highly oxidized when they are in contact with air. Complementary microstructural and magnetic characterizations of nanoparticles after hydrothermal treatment show unambiguously that they consist of magnetite with only a slight deviation from stoichiometry (δ ≈ 0.05), leading to Fe 2.95 O 4 .
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Citations
Cited by
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Wu, W., He, Q., & Jiang, C. (2008) · Nanoscale Research Letters · doi:10.1007/s11671-008-9174-9 · Cited by 2,300
Fundamentals and advances in magnetic hyperthermia
Périgo, E. A., Hemery, G., Sandre, O., Ortega, D., Garaio, E., Plazaola, F., & Teran, F. J. (2015) · Applied Physics Reviews · doi:10.1063/1.4935688 · Cited by 836
Organic Phase Syntheses of Magnetic Nanoparticles and Their Applications
Wu, L., Mendoza-Garcia, A., Li, Q., & Sun, S. (2016) · Chemical Reviews · doi:10.1021/acs.chemrev.5b00687 · Cited by 601
Magnetic Iron Oxide Nanoparticle (IONP) Synthesis to Applications: Present and Future
Ajinkya, N., Yu, X., Kaithal, P., Luo, H., Somani, P., & Ramakrishna, S. (2020) · Materials · doi:10.3390/ma13204644 · Cited by 362
Solvothermal Synthesis and Characterization of Fe3O4 and γ-Fe2O3 Nanoplates
Lu, J., Jiao, X., Chen, D., & Li, W. (2009) · The Journal of Physical Chemistry C · doi:10.1021/jp810583e · Cited by 308
Metadata
- Authors
- Daou, T. J., Pourroy, G., Bégin-Colin, S., Grenèche, J. M., Ulhaq-Bouillet, C., Legaré, P., Bernhardt, P., Leuvrey, C., & Rogez, G.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2006-08-04
- Volume
- 18
- Issue
- 18
- Pages
- 4399-4404
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2012892192
- Cited by
- 651
- References
- 0
- FWCI
- 13.02
- Type
- journal article
- Language
- en
- Open access
- closed
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- Daou, T. J., Pourroy, G., Bégin-Colin, S., Grenèche, J. M., Ulhaq-Bouillet, C., Legaré, P., Bernhardt, P., Leuvrey, C., & Rogez, G. (2006). Hydrothermal Synthesis of Monodisperse Magnetite Nanoparticles. Chemistry of Materials. https://doi.org/10.1021/cm060805r
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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