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Synthesis and Electrochemical Performance of Heteroatom-Incorporated Ordered Mesoporous Carbons
Abstract
Heteroatom-incorporated 2D ordered mesoporous carbons (OMCs) were fabricated via a one-pot organic−organic aqueous self-assembly approach, using resorcinol (R) and formaldehyde (F) as the carbon precursor and triblock copolymer Pluronic F127 as the mesoporous structure template. In this approach, RF resin, boric acid and/or phosphoric acid, and F127 underwent a self-assembly process under a strong acidic condition to form a polymer with ordered mesostructure, which was then carbonized at 800 °C in a nitrogen atmosphere to form B-incorporated, P-incorporated, or B, P-coincorporated OMCs. Nitrogen sorption, X-ray diffraction (XRD), and transmission electron microscopy (TEM) revealed that the heteroatom-incorporated OMCs possessed highly ordered mesoporous structures, uniform pore size distributions, and large surface areas ranging from 500 to 700 m 2 /g. The incorporation of heteroatoms effectively limited the framework shrinkage during the carbonization process, and simultaneously increased the surface oxygen groups in the carbons. The resulting heteroatom-incorporated OMCs exhibited superior electrochemical performances to nonincorporated counterpart when used as electrodes of supercapacitors.
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Mesoporous carbon materials: Synthesis and modification
Liang, C., Li, Z., & Dai, S. (2008) · Angewandte Chemie International Edition · doi:10.1002/anie.200702046 · Cited by 1,935
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Metadata
- Authors
- Zhao, X., Wang, A., Yan, J., Sun, G., Sun, L., & Zhang, T.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2010-09-13
- Volume
- 22
- Issue
- 19
- Pages
- 5463-5473
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2316902873
- Cited by
- 217
- References
- 1
- FWCI
- 7.56
- Type
- journal article
- Language
- en
- Open access
- closed
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