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Synthesis of Atomically Thin WO3 Sheets from Hydrated Tungsten Trioxide
Abstract
Atomically thin WO 3 is fabricated using a three-step process, involving wet-chemical synthesis of hydrated-WO 3, mechanical exfoliation of fundamental layers and dehydration by annealing at 300 °C. Atomic force microscopy reveals that the minimum resolvable thickness of the hydrated flakes to be ∼1.4 nm, which corresponds to the unit-cell height. The subsequent annealing temperature determines the degree of dehydration and thereby the crystallographic structure of the resultant WO 3 . The hydrated and dehydrated flakes are characterized by Raman spectroscopy to reveal spectroscopic fingerprints of flake thickness. Thin flakes are also shown to have higher propensity for lithium intercalation, which is also evidenced in Raman planar peak intensity.
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Cited by
Electronics and optoelectronics of two-dimensional transition metal dichalcogenides
Wang, Q. H., Kalantar-Zadeh, K., Kis, A., Coleman, J. N., & Strano, M. S. (2012) · Nature Nanotechnology · doi:10.1038/nnano.2012.193 · Cited by 16,374
Self-citationNanostructured Tungsten Oxide – Properties, Synthesis, and Applications
Zheng, H., Ou, J. Z., Strano, M. S., Kaner, R. B., Mitchell, A., & Kalantar‐zadeh, K. (2011) · Advanced Functional Materials · doi:10.1002/adfm.201002477 · Cited by 1,479
Self-citationElectrically-Transduced Chemical Sensors Based on Two-Dimensional Nanomaterials
Meng, Z., Stolz, R. M., Mendecki, L., & Mirica, K. A. (2019) · Chemical Reviews · doi:10.1021/acs.chemrev.8b00311 · Cited by 773
Li, H., Lu, G., Wang, Y., Yin, Z., Cong, C., He, Q., Wang, L., Ding, F., Yu, T., & Zhang, H. (2013) · Small · doi:10.1002/smll.201202919 · Cited by 659
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Huang, Z., Song, J., Pan, L., Zhang, X., Wang, L., & Zou, J. (2015) · Advanced Materials · doi:10.1002/adma.201501217 · Cited by 608
Metadata
- Authors
- Kalantar-zadeh, K., Vijayaraghavan, A., Ham, M.-H., Zheng, H., Breedon, M., & Strano, M. S.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2010-09-07
- Volume
- 22
- Issue
- 19
- Pages
- 5660-5666
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2044278655
- Cited by
- 242
- References
- 0
- FWCI
- 11.78
- Type
- journal article
- Language
- en
- Open access
- closed
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- Kalantar-zadeh, K., Vijayaraghavan, A., Ham, M.-H., Zheng, H., Breedon, M., & Strano, M. S. (2010). Synthesis of Atomically Thin WO3 Sheets from Hydrated Tungsten Trioxide. Chemistry of Materials. https://doi.org/10.1021/cm1019603
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