The DOI matches its Crossref record; 1 of the 1 references it cites were found in a registry or an index.
A Novel Wet Chemistry Approach for the Synthesis of Hybrid 2D Free-Floating Single or Multilayer Nanosheets of MS2@oleylamine (M═Mo, W)
Abstract
A new wet chemistry approach, based on low-temperature (360 °C) decomposition in oleylamine of single-source precursors containing both metal and sulfur, is proposed for the production of stable free-standing nanosheets of MoS 2 and WS 2 . The one-pot synthesis permits high-quality 2D nanosheet crystals of MoS 2 and WS 2 to be obtained with a modular number of nanolayers for units. The layered materials obtained are covered by a dynamic protective coating of oleylamine that stabilizes the suspension, avoids aggregation and oxidation phenomena, and could be easily functionalized with other molecules or nanosystems to introduce new properties to the hybrid organic–inorganic nanocomposite. The reaction products were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), attenuated total reflectance Fourier transform infrared spectroscopy (ART-FTIR), field emission scanning electron microscopy (FESEM), X-ray photoelectron spectroscopy (XPS), thermogravimetric analysis coupled with mass spectrometry (TG-MS), and dynamic light scattering (DLS) for particle size distribution (PSD).
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Citations
Cites
XPS studies of MoS2 formation from ammonium tetrathiomolybdate solutions
Wang, H. W., Skeldon, P., & Thompson, G. E. (1997) · Surface and Coatings Technology · doi:10.1016/s0257-8972(96)03186-6 · Cited by 302
Cited by
Synthesis of Large‐Area MoS2 Atomic Layers with Chemical Vapor Deposition
Lee, Y., Zhang, X., Zhang, W., Chang, M., Lin, C., Chang, K., Yu, Y., Wang, J. T., Chang, C., Li, L., et al. (2012) · Advanced Materials · doi:10.1002/adma.201104798 · Cited by 3,422
Gao, M.-R., Xu, Y.-F., Jiang, J., & Yu, S.-H. (2013) · Chemical Society Reviews · doi:10.1039/c2cs35310e · Cited by 1,610
Mahler, B., Hoepfner, V., Liao, K., & Ozin, G. A. (2014) · Journal of the American Chemical Society · doi:10.1021/ja506261t · Cited by 837
Chang, Y., Lin, C., Chen, T., Hsu, C., Lee, Y., Zhang, W., Wei, K., & Li, L. (2013) · Advanced Materials · doi:10.1002/adma.201202920 · Cited by 744
Second harmonic microscopy of monolayer MoS2
Kumar, N., Najmaei, S., Cui, Q., Ceballos, F., Ajayan, P. M., Lou, J., & Zhao, H. (2013) · Physical Review B · doi:10.1103/physrevb.87.161403 · Cited by 699
Metadata
- Authors
- Altavilla, C., Sarno, M., & Ciambelli, P.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2011-08-11
- Volume
- 23
- Issue
- 17
- Pages
- 3879-3885
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2314915452
- Cited by
- 317
- References
- 1
- FWCI
- 7.59
- Type
- journal article
- Language
- en
- Open access
- closed
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