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Conversion Reactions of Cadmium Chalcogenide Nanocrystal Precursors
Abstract
We survey the chemical reactions between common precursors used in the synthesis of metal chalcogenide nanocrystals and outline how they affect the mechanism and kinetics of nanocrystal growth. We emphasize syntheses of cadmium selenide and cadmium sulfide where a variety of metal and chalcogenide precursors have been explored, though this is supplemented by studies of zinc and lead chalcogenide formation where appropriate. This review is organized into three sections, highlighting kinetics, metal precursors, and chalcogenide precursors, respectively. Section I is dedicated to the role of precursor conversion as a source of monomers and the importance of the supply rate on nanocrystal nucleation and growth. Section II describes the structure and reactivity of cadmium carboxylates, phosphonates, and chalcogenolates. Section III describes the reaction chemistry of commonly employed chalcogenide precursors and the mechanisms by which they react with metal precursors.
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Cites
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Cited by
Anderson, N. C., Hendricks, M. P., Choi, J. J., & Owen, J. S. (2013) · Journal of the American Chemical Society · doi:10.1021/ja4086758 · Cited by 874
Self-citationThe Heat-Up Synthesis of Colloidal Nanocrystals
van Embden, J., Chesman, A. S. R., & Jasieniak, J. J. (2015) · Chemistry of Materials · doi:10.1021/cm5028964 · Cited by 414
Chemical Synthesis and Luminescence Applications of Colloidal Semiconductor Quantum Dots
Owen, J., & Brus, L. (2017) · Journal of the American Chemical Society · doi:10.1021/jacs.7b05267 · Cited by 369
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Metadata
- Authors
- García-Rodríguez, R., Hendricks, M. P., Cossairt, B. M., Liu, H., & Owen, J. S.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2013-03-06
- Volume
- 25
- Issue
- 8
- Pages
- 1233-1249
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2020766278
- Cited by
- 226
- References
- 5
- FWCI
- 7.55
- Type
- journal article
- Language
- en
- Open access
- closed
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- García-Rodríguez, R., Hendricks, M. P., Cossairt, B. M., Liu, H., & Owen, J. S. (2013). Conversion Reactions of Cadmium Chalcogenide Nanocrystal Precursors. Chemistry of Materials. https://doi.org/10.1021/cm3035642
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