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Synthesis and Characterization of Nanometer-Size Fe3O4 and γ-Fe2O3 Particles
Abstract
Synthesis of suspensions of nanosize particles of Fe3O4 was carried out in bulk aqueous solutions without the presence of surfactants. The Fe3O4 nanoparticles were oxidized to γ-Fe2O3 by direct aeration of the suspension at 100 °C. The shape and size distribution and crystallinity of the Fe3O4 nanoparticles were assessed by transmission electron microscopy and selected area electron diffraction. Very uniform and stable colloidal suspensions of the Fe3O4 nanoparticles in water could be synthesized. Oxidation of the colloidal system leads to γ-Fe2O3 nanoparticles of much larger size than Fe3O4.
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Citations
Cited by
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Wu, W., He, Q., & Jiang, C. (2008) · Nanoscale Research Letters · doi:10.1007/s11671-008-9174-9 · Cited by 2,300
Heavy metal removal from water/wastewater by nanosized metal oxides: A review
Hua, M., Zhang, S., Pan, B., Zhang, W., Lv, L., & Zhang, Q. (2012) · Journal of Hazardous Materials · doi:10.1016/j.jhazmat.2011.10.016 · Cited by 2,193
Shape Control of Semiconductor and Metal Oxide Nanocrystals through Nonhydrolytic Colloidal Routes
Jun, Y., Choi, J., & Cheon, J. (2006) · Angewandte Chemie International Edition · doi:10.1002/anie.200503821 · Cited by 1,123
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Louie, A. (2010) · Chemical Reviews · doi:10.1021/cr9003538 · Cited by 1,044
Metadata
- Authors
- Kang, Y. S., Risbud, S., Rabolt, J. F., & Stroeve, P.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 1996-01-01
- Volume
- 8
- Issue
- 9
- Pages
- 2209-2211
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W4242599454
- Cited by
- 1,068
- References
- 0
- FWCI
- 3.38
- Type
- journal article
- Language
- en
- Open access
- closed
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- Kang, Y. S., Risbud, S., Rabolt, J. F., & Stroeve, P. (1996). Synthesis and Characterization of Nanometer-Size Fe3O4 and γ-Fe2O3 Particles. Chemistry of Materials. https://doi.org/10.1021/cm960157j
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