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Base-Free Oxidation of Alcohols to Esters at Room Temperature and Atmospheric Conditions using Nanoscale Co-Based Catalysts
Abstract
The direct oxidation of alcohols to esters with molecular oxygen is an attractive and crucial process for the synthesis of fine chemicals. To date, the heterogeneous catalyst systems that have been identified are based on noble metals or have required the addition of base additives. Here, we show that Co nanoparticles embedded in nitrogen-doped graphite catalyze the aerobic oxidation of alcohols to esters at room temperature under base-free and atmospheric conditions. Our Co@C-N catalytic system features a broad substrate scope for aromatic and aliphatic alcohols as well as diols, giving their corresponding esters in good to excellent yields. This apparently environmentally benign process provides a new strategy with which to achieve selective oxidation of alcohols.
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Cites
Metal-organic framework materials as catalysts
Lee, J., Farha, O. K., Roberts, J., Scheidt, K. A., Nguyen, S. T., & Hupp, J. T. (2009) · Chemical Society Reviews · doi:10.1039/b807080f · Cited by 7,969
Catalytic Graphitization of Carbon Aerogels by Transition Metals
Maldonado-Hódar, F. J., Moreno-Castilla, C., Rivera-Utrilla, J., Hanzawa, Y., & Yamada, Y. (2000) · Langmuir · doi:10.1021/la991080r · Cited by 494
Cited by
Sun, M.-H., Huang, S.-Z., Chen, L.-H., Li, Y., Yang, X.-Y., Yuan, Z.-Y., & Su, B.-L. (2016) · Chemical Society Reviews · doi:10.1039/c6cs00135a · Cited by 1,454
Self-citationJiao, L., Zhou, Y.-X., & Jiang, H.-L. (2016) · Chemical Science · doi:10.1039/c5sc04425a · Cited by 798
He, L., Weniger, F., Neumann, H., & Beller, M. (2016) · Angewandte Chemie International Edition · doi:10.1002/anie.201603198 · Cited by 618
The recent development of efficient Earth-abundant transition-metal nanocatalysts
Wang, D., & Astruc, D. (2017) · Chemical Society Reviews · doi:10.1039/c6cs00629a · Cited by 608
Metal organic frameworks as precursors for the manufacture of advanced catalytic materials
Oar-Arteta, L., Wezendonk, T., Sun, X., Kapteijn, F., & Gascon, J. (2017) · Materials Chemistry Frontiers · doi:10.1039/c7qm00007c · Cited by 361
Metadata
- Authors
- Zhong, W., Liu, H., Bai, C., Liao, S., & Li, Y.
- Venue
- ACS Catalysis
- Publisher
- American Chemical Society (ACS)
- Published
- 2015-02-20
- Volume
- 5
- Issue
- 3
- Pages
- 1850-1856
- ISSN
- 2155-5435 (ISSN-L)
- OpenAlex
- W2324299205
- Cited by
- 325
- References
- 2
- FWCI
- 16.93
- Type
- journal article
- Language
- en
- Open access
- closed
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- Zhong, W., Liu, H., Bai, C., Liao, S., & Li, Y. (2015). Base-Free Oxidation of Alcohols to Esters at Room Temperature and Atmospheric Conditions using Nanoscale Co-Based Catalysts. ACS Catalysis. https://doi.org/10.1021/cs502101c
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