The Adsorption of SO 2 by Zeolites Synthesized from Fly Ash
Abstract
Zeolites X, Y, and Na-P1 (90 °C) and analcime and sodalite (150 °C) were synthesized from Class F fly ash using 3 M sodium hydroxide solutions and autogenous pressures. The partially zeolitized fly ashes were dried overnight in air at room temperature and then characterized using X-ray diffraction and SEM. On occasion, a few samples were dried to constant weight for an additional 8−10 min in a microwave oven to remove bound water as well. The dried samples were evaluated for their ability to adsorb sulfur dioxide (SO 2 ) from a simulated stack gas containing ∼2000 ppm SO 2 . Determinations were made in real time using a UV/vis spectrophotometer followed by a total sulfur analysis of the “loaded” samples once testing was complete. Breakthrough curves indicate that the zeolites in the samples are able to remove all of the SO 2 in the simulated flue gas (zero SO 2 emission) for varying periods of time, and that the actual amount of SO 2 removed by the zeolite depended on the type and degree of “dryness” of the zeolite or zeolite-like material present. For example, a 7 day 150 °C cured sample containing analcime and sodalite was able to adsorb 6−7 mg of SO 2 per gram of sample regardless of the source of the fly ash, whereas a 90 °C cured sample containing X, Y, and Na-P1 was significantly less efficient.
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The largest SO2 adsorption capacity at room temperature among zeolites synthesized from fly ash was given by a mixture of sodalite and analcime.
“found that the largest SO2 adsorption capacity at room temperature was given by a mixture of sodalite and analcime.616”
From Zeolites in Adsorption Processes: State of the Art and Future Prospects (2022) · cites this paper as [616]
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- Authors
- Srinivasan, A., & Grutzeck, M. W.
- Affiliations
- Pennsylvania State University (US)
- Venue
- Environmental Science & Technology
- Publisher
- American Chemical Society (ACS)
- Published
- 1999-03-31
- Volume
- 33
- Issue
- 9
- Pages
- 1464-1469
- ISSN
- 0013-936X (ISSN-L)
- 1520-5851
- OpenAlex
- W2090399743
- Cited by
- 147
- References
- 15
- Citations by year
- 2026: 5 · 2025: 5 · 2024: 5 · 2023: 7 · 2022: 6 · 2021: 13 · 2020: 7 · 2019: 6 · 2018: 5 · 2017: 7 · 2016: 8 · 2015: 2 · 2014: 5 · 2013: 8 · 2012: 5
- FWCI
- 12.82
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- Environmental Science & Technology (publishedVersion)
- Funders
- U.S. Department of Energy
- Topics
- Physical Sciences › Engineering › Mechanical Engineering › Industrial Gas Emission Control
- Physical Sciences › Chemistry › Inorganic Chemistry › Zeolite Catalysis and Synthesis
- Physical Sciences › Engineering › Mechanical Engineering › Carbon Dioxide Capture Technologies
- Keywords
- SO2 adsorption, zeolites, fly ash, zeolite synthesis, flue gas desulfurization, zeolite X, zeolite Y, Na-P1 zeolite, analcime, sodalite, microwave drying, breakthrough curves, stack gas
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