Cited by 64ZnO doping and propertiesNanowire Synthesis and ApplicationsLaser-Ablation Synthesis of Nanoparticles

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Fast Synthesis of ZnO Nanostructures by Laser-Induced Decomposition of Zinc Acetylacetonate

Fauteux, Christian, Longtin, Rémi, Pegna, Joseph, Therriault, Daniel·2007·Inorganic Chemistry

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Abstract

A CO2 laser (lambda = 10.6 microm) was used to heat a solution of water and alcohol saturated by Zn(AcAc)2 on a fused quartz substrate in open air. After only a few seconds of irradiation, various zinc oxide (ZnO) nanostructures including nanorods and nanowires are formed near the center of the irradiated zone, surrounded by a porous thin film of ZnO nanoparticles. The type of structures produced and their localization on the substrate can be varied by selecting adequate irradiation time and laser power ranges. The deposits have been analyzed using SEM, TEM, EDS, XRD, and Raman spectroscopy, revealing that the nanorods (aspect ratio ~6) and nanowires (aspect ratio ~94) are single-crystalline structures which grow along the c axis of wurtzite ZnO. The nanoparticles are also single-crystalline and have an average diameter of 16 nm. A qualitative model for nanostructure growth is proposed, based on previous studies of aqueous solution and hydrothermal processing.

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Authors: Fauteux, C., Longtin, R., Pegna, J., & Therriault, D.
Affiliations: Research Center for High Performance Polymer and Composite Systems (CA)
Corresponding author: Fauteux, Christian
ORCID: Pegna, Joseph
Therriault, Daniel
Venue: Inorganic Chemistry
Publisher: American Chemical Society (ACS)
Published: 2007-11-21
Volume: 46
Issue: 26
Pages: 11036-11047
ISSN: 0020-1669 (ISSN-L)
1520-510X
DOI: 10.1021/ic700915z
OpenAlex: W1985183096
Cited by: 63
References: 60
Citations by year: 2026: 1 · 2025: 1 · 2024: 2 · 2023: 1 · 2022: 2 · 2021: 2 · 2020: 2 · 2019: 4 · 2018: 6 · 2017: 6 · 2016: 2 · 2015: 1 · 2014: 4 · 2013: 4 · 2012: 3
FWCI: 2.76
Type: journal article
Language: en
Open access: closed
Locations: Inorganic Chemistry (publishedVersion)
PubMed (publishedVersion)
PolyPublie (École Polytechnique de Montréal) (submittedVersion)
Topics: Physical Sciences › Materials Science › Materials Chemistry › ZnO doping and properties
Physical Sciences › Materials Science › Electronic, Optical and Magnetic Materials › Nanowire Synthesis and Applications
Physical Sciences › Materials Science › Materials Chemistry › Laser-Ablation Synthesis of Nanoparticles
Keywords: ZnO nanostructures, laser-induced decomposition, zinc acetylacetonate, CO2 laser, nanorods, nanowires, zinc oxide nanoparticles, single-crystalline nanostructures, wurtzite structure, aqueous processing, hydrothermal treatment

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Fast Synthesis of ZnO Nanostructures by Laser-Induced Decomposition of Zinc Acetylacetonate

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