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Discovery of Exceptionally Efficient Catalysts for Solvent-Free Enantioselective Hetero-Diels−Alder Reaction
Abstract
Combinatorial coordination chemistry strategy combined with high-throughput screening techniques has been successfully applied to engineering practical enantioselective catalysts for asymmetric hetero-Diels-Alder reaction. The reaction of Danishefsky's diene with a variety of aldehydes can be carried out with 0.1-0.005 mol % of H4-BINOL/Ti/H4-BINOL or H4-BINOL/Ti/H8-BINOL catalysts at room temperature under solvent- and MS-free conditions to afford dihydropyrone derivatives with up to quantitative yield and 99.8% ee.
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Berrisford, D. J., Bolm, C., & Sharpless, K. B. (1995) · Angewandte Chemie International Edition in English · doi:10.1002/anie.199510591 · Cited by 606
Pandiaraju, S., Chen, G., Lough, A. J., & Yudin, A. K. (2001) · Journal of the American Chemical Society · doi:10.1021/ja0039942 · Cited by 73
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Metadata
- Authors
- Long, J., Hu, J., Shen, X., Ji, B., & Ding, K.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2001-12-06
- Volume
- 124
- Issue
- 1
- Pages
- 10-11
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W1976165583
- Cited by
- 296
- References
- 2
- FWCI
- 24.07
- Type
- journal article
- Language
- en
- Open access
- closed
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