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Understanding the Role of Oxidative Etching in the Polyol Synthesis of Pd Nanoparticles with Uniform Shape and Size
Abstract
Uniform cubooctahedral nanoparticles of Pd were synthesized using a modified polyol process. Like the silver system, the Pd nanoparticles underwent dissolution due to oxidative etching by Cl-/O2. In the early stage of etching, the twinned particles in a sample were selectively removed to leave behind uniform, single-crystal cubooctahedra. If the etching was allowed to continue, the single-crystal cubooctahedra were also attacked and partially dissolved. Understanding the role of oxidative etching is critical to the achievement of both uniform shape and size.
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Metadata
- Authors
- Xiong, Y., Chen, J., Wiley, B., Xia, Y., Aloni, S., & Yin, Y.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2005-05-03
- Volume
- 127
- Issue
- 20
- Pages
- 7332-7333
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W1980378453
- Cited by
- 451
- References
- 21
- FWCI
- 12.82
- Type
- journal article
- Language
- en
- Open access
- closed
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