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AAB-Sequence Living Radical Chain Copolymerization of Naturally Occurring Limonene with Maleimide: An End-to-End Sequence-Regulated Copolymer
Abstract
Sequence control in chain-growth polymerization is still one of the most challenging topics in synthetic polymer chemistry in contrast to natural macromolecules with completely sequence-regulated structures like proteins and DNA. Here, we report the quantitative and highly selective 1:2 sequence-regulated radical copolymerization of naturally occurring (+)-d-limonene (L) and a maleimide (M) in fluoroalcohol giving chiral copolymers with high glass transition temperatures (220-250 degrees C) originating from the specific rigid cyclic structures of the monomers. Furthermore, the combination with a reversible addition-fragmentation chain transfer (RAFT) agent (C-S) via the controlled/living radical polymerization resulted in end-to-end sequence-regulated copolymers [C-(M-M-L)(n)-M-S] with both highly sequenced chain ends and main-chain repeating units as well as controlled molecular weights.
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Odian, G. (2004) · doi:10.1002/047147875x · Cited by 7,158
(1985) · doi:10.1007/978-1-4757-9139-6 · Cited by 227
Cited by
Isikgor, F. H., & Becer, C. R. (2015) · Polymer Chemistry · doi:10.1039/c5py00263j · Cited by 2,775
Lutz, J.-F., Ouchi, M., Liu, D. R., & Sawamoto, M. (2013) · Science · doi:10.1126/science.1238149 · Cited by 1,381
Controlled Polymerization of Next-Generation Renewable Monomers and Beyond
Yao, K., & Tang, C. (2013) · Macromolecules · doi:10.1021/ma3019574 · Cited by 485
Metadata
- Authors
- Satoh, K., Matsuda, M., Nagai, K., & Kamigaito, M.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2010-06-30
- Volume
- 132
- Issue
- 29
- Pages
- 10003-10005
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W2084555720
- Cited by
- 275
- References
- 2
- FWCI
- 10.42
- Type
- journal article
- Language
- en
- Open access
- closed
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