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Reductive Electrosynthesis of Crystalline Metal–Organic Frameworks
Open accessAbstract
Electroreduction of oxoanions affords hydroxide equivalents that induce selective deposition of crystalline metal-organic frameworks (MOFs) on conductive surfaces. The method is illustrated by cathodic electrodeposition of Zn(4)O(BDC)(3) (MOF-5; BDC = 1,4-benzenedicarboxylate), which is deposited at room temperature in only 15 min under cathodic potential. Although many crystalline phases are known in the Zn(2+)/BDC(2-) system, MOF-5 is the only observed crystalline MOF phase under these conditions. This fast and mild method of synthesizing MOFs is amenable to direct surface functionalization and could impact applications requiring conformal coatings of microporous MOFs, such as gas separation membranes and electrochemical sensors.
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Sumida, K., Horike, S., Kaye, S. S., Herm, Z. R., Queen, W. L., Brown, C. M., Grandjean, F., Long, G. J., Dailly, A., & Long, J. R. (2010) · Chemical Science · doi:10.1039/c0sc00179a · Cited by 347
Electrochemical Biomineralization: The Deposition of Calcite with Chiral Morphologies
Kulp, E. A., & Switzer, J. A. (2007) · Journal of the American Chemical Society · doi:10.1021/ja076303b · Cited by 43
Cited by
MOF positioning technology and device fabrication
Falcaro, P., Ricco, R., Doherty, C. M., Liang, K., Hill, A. J., & Styles, M. J. (2014) · Chem. Soc. Rev. · doi:10.1039/c4cs00089g · Cited by 710
Li, W.-J., Tu, M., Cao, R., & Fischer, R. A. (2016) · Journal of Materials Chemistry A · doi:10.1039/c6ta02118b · Cited by 283
Metadata
- Authors
- Li, M., & Dincă, M.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2011-07-29
- Volume
- 133
- Issue
- 33
- Pages
- 12926-12929
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W2091480522
- Cited by
- 311
- References
- 2
- FWCI
- 7.72
- Type
- journal article
- Language
- en
- Open access
- green
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