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A 2D Covalent Organic Framework with 4.7-nm Pores and Insight into Its Interlayer Stacking
Abstract
Two-dimensional layered covalent organic frameworks (2D COFs) organize π-electron systems into ordered structures ideal for exciton and charge transport and exhibit permanent porosity available for subsequent functionalization. A 2D COF with the largest pores reported to date was synthesized by condensing 2,3,6,7,10,11-hexahydroxytriphenylene (HHTP) and 4,4'-diphenylbutadiynebis(boronic acid) (DPB). The COF was prepared as both a high surface area microcrystalline powder as well as a vertically oriented thin film on a transparent single-layer graphene/fused silica substrate. Complementary molecular dynamics and density functional theory calculations provide insight into the interlayer spacing of the COF and suggest that adjacent layers are horizontally offset by 1.7-1.8 Å, in contrast to the eclipsed AA stacking typically proposed for these materials.
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Sing, K. S. W. (1985) · Pure and Applied Chemistry · doi:10.1351/pac198557040603 · Cited by 24,485
Cited by
Liu, R., Tan, K. T., Gong, Y., Chen, Y., Li, Z., Xie, S., He, T., Lu, Z., Yang, H., & Jiang, D. (2021) · Chemical Society Reviews · doi:10.1039/d0cs00620c · Cited by 1,083
Wang, H., Zeng, Z., Xu, P., Li, L., Zeng, G., Xiao, R., Tang, Z., Huang, D., Tang, L., Lai, C., et al. (2019) · Chemical Society Reviews · doi:10.1039/c8cs00376a · Cited by 804
Beuerle, F., & Gole, B. (2018) · Angewandte Chemie International Edition · doi:10.1002/anie.201710190 · Cited by 528
Design and fabrication of mesoporous heterogeneous basic catalysts
Sun, L.-B., Liu, X.-Q., & Zhou, H.-C. (2015) · Chemical Society Reviews · doi:10.1039/c5cs00090d · Cited by 386
Metadata
- Authors
- Spitler, E. L., Koo, B. T., Novotney, J. L., Colson, J. W., Uribe-Romo, F. J., Gutierrez, G. D., Clancy, P., & Dichtel, W. R.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2011-11-11
- Volume
- 133
- Issue
- 48
- Pages
- 19416-19421
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W2332785792
- Cited by
- 386
- References
- 1
- FWCI
- 10.22
- Type
- journal article
- Language
- en
- Open access
- closed
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- Spitler, E. L., Koo, B. T., Novotney, J. L., Colson, J. W., Uribe-Romo, F. J., Gutierrez, G. D., Clancy, P., & Dichtel, W. R. (2011). A 2D Covalent Organic Framework with 4.7-nm Pores and Insight into Its Interlayer Stacking. Journal of the American Chemical Society. https://doi.org/10.1021/ja206242v
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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