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Opening ZIF-8: A Catalytically Active Zeolitic Imidazolate Framework of Sodalite Topology with Unsubstituted Linkers
Abstract
A zeolitic imidazolate framework material of SOD topology possessing primarily unsubstituted imidazolate (im) linkers has been synthesized via solvent-assisted linker exchange (SALE) of ZIF-8. The structure of the new material, SALEM-2, has been confirmed through (1)H NMR and powder and single-crystal X-ray diffraction. SALEM-2 is the first example of a porous Zn(im)(2) ZIF possessing a truly zeolitic topology that can be obtained in bulk quantities. Upon treatment with n-butyllithium, the open analogue exhibits Brønsted base catalysis that cannot be accomplished by the parent material ZIF-8. Additionally, it displays a different size cutoff for uptake and release of molecular guests than does ZIF-8.
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Horike, S., Shimomura, S., & Kitagawa, S. (2009) · Nature Chemistry · doi:10.1038/nchem.444 · Cited by 2,486
Tan, J. C., Bennett, T. D., & Cheetham, A. K. (2010) · Proceedings of the National Academy of Sciences · doi:10.1073/pnas.1003205107 · Cited by 552
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Zhuang, J., Kuo, C.-H., Chou, L.-Y., Liu, D.-Y., Weerapana, E., & Tsung, C.-K. (2014) · ACS Nano · doi:10.1021/nn406590q · Cited by 873
Best Practices for the Synthesis, Activation, and Characterization of Metal–Organic Frameworks
Howarth, A. J., Peters, A. W., Vermeulen, N. A., Wang, T. C., Hupp, J. T., & Farha, O. K. (2017) · Chemistry of Materials · doi:10.1021/acs.chemmater.6b02626 · Cited by 746
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Metadata
- Authors
- Karagiaridi, O., Lalonde, M. B., Bury, W., Sarjeant, A. A., Farha, O. K., & Hupp, J. T.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2012-10-31
- Volume
- 134
- Issue
- 45
- Pages
- 18790-18796
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W2075429271
- Cited by
- 473
- References
- 2
- FWCI
- 19.40
- Type
- journal article
- Language
- en
- Open access
- closed
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- Karagiaridi, O., Lalonde, M. B., Bury, W., Sarjeant, A. A., Farha, O. K., & Hupp, J. T. (2012). Opening ZIF-8: A Catalytically Active Zeolitic Imidazolate Framework of Sodalite Topology with Unsubstituted Linkers. Journal of the American Chemical Society. https://doi.org/10.1021/ja308786r
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