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Synthesis of Graphdiyne Nanowalls Using Acetylenic Coupling Reaction
Abstract
Synthesizing graphdiyne with a well-defined structure is a great challenge. We reported herein a rational approach to synthesize graphdiyne nanowalls using a modified Glaser-Hay coupling reaction. Hexaethynylbenzene and copper plate were selected as monomer and substrate, respectively. By adjusting the ratio of added organic alkali along with the amount of monomer, the proper amount of copper ions was dissolved into the solution, thus forming catalytic reaction sites. With a rapid reaction rate of Glaser-Hay coupling, graphdiyne grew vertically at these sites first, and then with more copper ions dissolved, uniform graphdiyne nanowalls formed on the surface of copper substrate. Raman spectra, UV-vis spectra, and HRTEM results confirmed the features of graphdiyne. These graphdiyne nanowalls also exhibited excellent and stable field-emission properties.
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Kroto, H. W., Allaf, A. W., & Balm, S. P. (1991) · Chemical Reviews · doi:10.1021/cr00006a005 · Cited by 1,088
Cited by
Interface-Assisted Synthesis of 2D Materials: Trend and Challenges
Dong, R., Zhang, T., & Feng, X. (2018) · Chemical Reviews · doi:10.1021/acs.chemrev.8b00056 · Cited by 710
Yin, X., Wang, H., Tang, S., Lu, X., Shu, M., Si, R., & Lu, T. (2018) · Angewandte Chemie International Edition · doi:10.1002/anie.201804817 · Cited by 594
Highly Efficient and Selective Generation of Ammonia and Hydrogen on a Graphdiyne-Based Catalyst
Hui, L., Xue, Y., Yu, H., Liu, Y., Fang, Y., Xing, C., Huang, B., & Li, Y. (2019) · Journal of the American Chemical Society · doi:10.1021/jacs.9b03004 · Cited by 587
Self-citationZeng, M., Xiao, Y., Liu, J., Yang, K., & Fu, L. (2018) · Chemical Reviews · doi:10.1021/acs.chemrev.7b00633 · Cited by 574
2D graphdiyne: An emerging carbon material
Fang, Y., Liu, Y., Qi, L., Xue, Y., & Li, Y. (2022) · Chemical Society Reviews · doi:10.1039/d1cs00592h · Cited by 520
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Metadata
- Authors
- Zhou, J., Gao, X., Liu, R., Xie, Z., Yang, J., Zhang, S., Zhang, G., Liu, H., Li, Y., Zhang, J., & Liu, Z.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2015-06-10
- Volume
- 137
- Issue
- 24
- Pages
- 7596-7599
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W2416839441
- Cited by
- 599
- References
- 1
- FWCI
- 16.39
- Type
- journal article
- Language
- en
- Open access
- closed
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- Zhou, J., Gao, X., Liu, R., Xie, Z., Yang, J., Zhang, S., Zhang, G., Liu, H., Li, Y., Zhang, J., & Liu, Z. (2015). Synthesis of Graphdiyne Nanowalls Using Acetylenic Coupling Reaction. Journal of the American Chemical Society. https://doi.org/10.1021/jacs.5b04057
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