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Purification and Characterization of Single-Wall Carbon Nanotubes
Abstract
A purification method has been developed that provides for the removal of metal catalysts and impurity carbon from laser-oven-grown single-wall carbon nanotube (SWNT) material. The oxidation rate of SWNTs in air at elevated temperatures is correlated to the metal content of the sample. Sample purity is documented with SEM, TEM, electron microprobe analysis, Raman, and UV−vis−near-IR. We also note that the relative intensity of the electronic transitions in the near-infrared to the continuum absorption at 400 nm in the UV serves as a useful monitor of the perturbation of the sidewall π-electron density of SWNTs due to sidewall substitution and/or oxidation.
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Citations
Cited by
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Adsorptive removal of dyes from aqueous solution onto carbon nanotubes: A review
Gupta, V. K., Kumar, R., Nayak, A., Saleh, T. A., & Barakat, M. A. (2013) · Advances in Colloid and Interface Science · doi:10.1016/j.cis.2013.03.003 · Cited by 1,253
Donaldson, K., Aitken, R., Tran, L., Stone, V., Duffin, R., Forrest, G., & Alexander, A. (2006) · Toxicological Sciences · doi:10.1093/toxsci/kfj130 · Cited by 1,167
Thermal conductivity of polymers and polymer nanocomposites
Huang, C., Qian, X., & Yang, R. (2018) · Materials Science and Engineering: R: Reports · doi:10.1016/j.mser.2018.06.002 · Cited by 909
The degree and kind of agglomeration affect carbon nanotube cytotoxicity
WICK, P., MANSER, P., LIMBACH, L., DETTLAFFWEGLIKOWSKA, U., KRUMEICH, F., ROTH, S., STARK, W., & BRUININK, A. (2007) · Toxicology Letters · doi:10.1016/j.toxlet.2006.08.019 · Cited by 818
Metadata
- Authors
- Chiang, I. W., Brinson, B. E., Smalley, R. E., Margrave, J. L., & Hauge, R. H.
- Venue
- The Journal of Physical Chemistry B
- Publisher
- American Chemical Society (ACS)
- Published
- 2001-01-12
- Volume
- 105
- Issue
- 6
- Pages
- 1157-1161
- ISSN
- 1520-5207 (ISSN-L)
- 1520-6106
- OpenAlex
- W2025702332
- Cited by
- 544
- References
- 0
- FWCI
- 23.99
- Type
- journal article
- Language
- en
- Open access
- closed
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- Chiang, I. W., Brinson, B. E., Smalley, R. E., Margrave, J. L., & Hauge, R. H. (2001). Purification and Characterization of Single-Wall Carbon Nanotubes. The Journal of Physical Chemistry B. https://doi.org/10.1021/jp003453z
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
