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Spectroelectrochemistry of Nanostructured NiO
Open accessAbstract
Transparent nanostructured NiO electrodes have been prepared by heating Ni(OH) 2 sol−gel films at a temperature of 300−320 °C. Nanostructured NiO (bunsenite) behaves as a p-type semiconductor and has an indirect band gap of 3.55 eV. It shows a strong anodic electrochromic effect, as it changes color from transparent to brown-black upon application of positive potentials. This effect is caused by oxidation of Ni atoms located at the NiO/electrolyte interface. Electrochemical oxidation reactions are highly reversible in both aqueous and nonaqueous electrolytes. In aqueous electrolyte, the half-potentials show a Nernstian pH dependence, whereas in nonaqueous electrolytes, the type of cation present determines the shape and position of the cyclic voltammogram.
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Metadata
- Authors
- Boschloo, G., & Hagfeldt, A.
- Venue
- The Journal of Physical Chemistry B
- Publisher
- American Chemical Society (ACS)
- Published
- 2001-03-27
- Volume
- 105
- Issue
- 15
- Pages
- 3039-3044
- ISSN
- 1520-5207 (ISSN-L)
- 1520-6106
- OpenAlex
- W2022739007
- Cited by
- 385
- References
- 10
- FWCI
- 5.58
- Type
- journal article
- Language
- en
- Open access
- green
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