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Sonochemical Synthesis of Mesoporous Iron Oxide and Accounts of Its Magnetic and Catalytic Properties
Abstract
Synthesis of mesoporous iron oxides has been reported using a sonochemical technique. Iron(III) ethoxide was used as an inorganic precursor and CTAB as an organic structure directing agent. After sonication the surfactant was removed by calcination and solvent extraction methods. FTIR spectra demonstrated the removal of the surfactant from the pores of the mesoporous iron oxide. The calcinated material was characterized by XRD, TEM, TGA, and BET surface area measurements. The surface area after solvent extraction is found to be 274 m 2 /g. The magnetic and catalytic properties of the materials have been studied. The as-prepared amorphous Fe 2 O 3 has shown a paramagnetic behavior, while after calcination at 350 °C it changes to γ-Fe 2 O 3 with good magnetic properties. The catalytic activity of mesoporous iron oxide was studied in the reaction of cyclohexane oxidation under mild conditions. The mesoporous Fe 2 O 3 catalyst has shown high conversion of cyclohexane into cyclohexanone and cyclohexanol, with a high selectivity.
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Cites
Sing, K. S. W. (1985) · Pure and Applied Chemistry · doi:10.1351/pac198557040603 · Cited by 24,485
Cited by
Cao, S.-W., & Zhu, Y.-J. (2010) · Nanoscale Research Letters · doi:10.1007/s11671-010-9742-7 · Cited by 2,357
Amorphous Iron(III) OxideA Review
Machala, L., Zboril, R., & Gedanken, A. (2007) · The Journal of Physical Chemistry B · doi:10.1021/jp064992s · Cited by 299
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Metadata
- Authors
- Srivastava, D. N., Perkas, N., Gedanken, A., & Felner, I.
- Venue
- The Journal of Physical Chemistry B
- Publisher
- American Chemical Society (ACS)
- Published
- 2002-01-17
- Volume
- 106
- Issue
- 8
- Pages
- 1878-1883
- ISSN
- 1520-5207 (ISSN-L)
- 1520-6106
- OpenAlex
- W2026695706
- Cited by
- 204
- References
- 1
- FWCI
- 5.61
- Type
- journal article
- Language
- en
- Open access
- closed
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- Srivastava, D. N., Perkas, N., Gedanken, A., & Felner, I. (2002). Sonochemical Synthesis of Mesoporous Iron Oxide and Accounts of Its Magnetic and Catalytic Properties. The Journal of Physical Chemistry B. https://doi.org/10.1021/jp015532w
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