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On the Shape of the Mesopores in Zeolite Y: A Three-Dimensional Transmission Electron Microscopy Study Combined with Texture Analysis
Open accessAbstract
The shape of the mesopores in a series of Y zeolites modified with different postsynthesis treatments was investigated. A combination of 3D-TEM (3D-TEM = three-dimensional transmission electron microscopy) with texture analysis (nitrogen physisorption and mercury porosimetry) enabled us to discriminate between cylindrical mesopores and mesoporous cavities inside the zeolite that are connected to the external surface via micropores. A large part of the mesopores in steamed and acid leached zeolite Y proved to be cavities, although the cylindrical mesopores in these samples account for the majority of the mesopore volume. Only after special hydrothermal treatments a zeolite Y with almost exclusively interconnected cylindrical mesopores is obtained.
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Cited by
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Chen, L.-H., Sun, M.-H., Wang, Z., Yang, W., Xie, Z., & Su, B.-L. (2020) · Chemical Reviews · doi:10.1021/acs.chemrev.0c00016 · Cited by 724
Tailored crystalline microporous materials by post-synthesis modification
Valtchev, V., Majano, G., Mintova, S., & Pérez-Ramírez, J. (2013) · Chem. Soc. Rev. · doi:10.1039/c2cs35196j · Cited by 478
Realizing the Commercial Potential of Hierarchical Zeolites: New Opportunities in Catalytic Cracking
Li, K., Valla, J., & Garcia‐Martinez, J. (2014) · ChemCatChem · doi:10.1002/cctc.201300345 · Cited by 470
Verboekend, D., Nuttens, N., Locus, R., Van Aelst, J., Verolme, P., Groen, J. C., Pérez-Ramírez, J., & Sels, B. F. (2016) · Chemical Society Reviews · doi:10.1039/c5cs00520e · Cited by 355
Mesopore quality determines the lifetime of hierarchically structured zeolite catalysts
Milina, M., Mitchell, S., Crivelli, P., Cooke, D., & Pérez-Ramírez, J. (2014) · Nature Communications · doi:10.1038/ncomms4922 · Cited by 351
Engineering Zeolites for Catalytic Cracking to Light Olefins
Blay, V., Louis, B., Miravalles, R., Yokoi, T., Peccatiello, K. A., Clough, M., & Yilmaz, B. (2017) · ACS Catalysis · doi:10.1021/acscatal.7b02011 · Cited by 277
Factors that Determine Zeolite Stability in Hot Liquid Water
Zhang, L., Chen, K., Chen, B., White, J. L., & Resasco, D. E. (2015) · Journal of the American Chemical Society · doi:10.1021/jacs.5b07398 · Cited by 208
Metadata
- Authors
- Janssen, A. H., Koster, A. J., & de Jong, K. P.
- Venue
- The Journal of Physical Chemistry B
- Publisher
- American Chemical Society (ACS)
- Published
- 2002-10-24
- Volume
- 106
- Issue
- 46
- Pages
- 11905-11909
- ISSN
- 1520-5207 (ISSN-L)
- 1520-6106
- OpenAlex
- W2126706966
- Cited by
- 229
- References
- 0
- FWCI
- 3.80
- Type
- journal article
- Language
- en
- Open access
- green
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