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Interaction between Lithium Amide and Lithium Hydride
Abstract
Pure lithium amide (LiNH 2 ) decomposes to lithium imide and ammonia at temperatures above 300 °C. Lithium hydride, on the other hand, liberates hydrogen at temperatures above 550 °C. By thoroughly mixing these two substances and conducting temperature-programmed desorption (TPD), we noticed that hydrogen was produced at temperatures around 150 °C. Combined thermogravimetric (TG), X-ray diffraction (XRD), and infrared (IR) analysis revealed that lithium amide would react with lithium hydride and convert to hydrogen and lithium imide (or Li-rich imide). The reaction mechanism was investigated by isotopic exchange.
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Citations
Cited by
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Wang, P., Chang, F., Gao, W., Guo, J., Wu, G., He, T., & Chen, P. (2017) · Nature Chemistry · doi:10.1038/nchem.2595 · Cited by 711
Self-citationVajo, J. J., Mertens, F., Ahn, C. C., Bowman, R. C., & Fultz, B. (2004) · The Journal of Physical Chemistry B · doi:10.1021/jp040060h · Cited by 477
Ternary Imides for Hydrogen Storage
Xiong, Z., Wu, G., Hu, J., & Chen, P. (2004) · Advanced Materials · doi:10.1002/adma.200400571 · Cited by 423
Self-citationHydrogen Storage Materials for Mobile and Stationary Applications: Current State of the Art
Lai, Q., Paskevicius, M., Sheppard, D. A., Buckley, C. E., Thornton, A. W., Hill, M. R., Gu, Q., Mao, J., Huang, Z., Liu, H. K., et al. (2015) · ChemSusChem · doi:10.1002/cssc.201500231 · Cited by 414
Mechanochemical synthesis of hydrogen storage materials
Huot, J., Ravnsbæk, D. B., Zhang, J., Cuevas, F., Latroche, M., & Jensen, T. R. (2013) · Progress in Materials Science · doi:10.1016/j.pmatsci.2012.07.001 · Cited by 406
Thermodynamic and kinetic investigations of the hydrogen storage in the Li–Mg–N–H system
Xiong, Z., Hu, J., Wu, G., Chen, P., Luo, W., Gross, K., & Wang, J. (2005) · Journal of Alloys and Compounds · doi:10.1016/j.jallcom.2005.02.010 · Cited by 276
Self-citationComplex hydrides for energy storage, conversion, and utilization
He, T., Cao, H., & Chen, P. (2019) · Advanced Materials · doi:10.1002/adma.201902757 · Cited by 256
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Metadata
- Authors
- Chen, P., Xiong, Z., Luo, J., Lin, J., & Tan, K. L.
- Venue
- The Journal of Physical Chemistry B
- Publisher
- American Chemical Society (ACS)
- Published
- 2003-09-10
- Volume
- 107
- Issue
- 39
- Pages
- 10967-10970
- ISSN
- 1520-5207 (ISSN-L)
- 1520-6106
- OpenAlex
- W2060303393
- Cited by
- 415
- References
- 0
- FWCI
- 13.35
- Type
- journal article
- Language
- en
- Open access
- closed
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