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Cited by 233

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MoS2 Nanostructures: Synthesis and Electrochemical Mg2+ Intercalation

Li, Xiao-Lin, Li, Ya-Dong·2004·The Journal of Physical Chemistry B

Abstract

MoS 2 nanostructures including hollow-cage fullerene-like particles, fibrous floccus, and spherical nanovesicles have been successfully synthesized by designed solution chemical reactions of Na 2 MoO 4 and sulfurization reagents such as CS 2, Na 2 S, CH 3 CSNH 2, CSN 2 H 4, and KSCN etc. Possible redox reaction routes have been proposed on the basis of the experimental facts. We have investigated the electrochemical properties of annealed MoS 2 samples finding that Mg 2+ ions showed better reversibly intercalation/deintercalation cycles in as-synthesized MoS 2 nanostructures than in bluk MoS 2 samples. The solution product of MoS 2 and their high-temperature annealing samples were characterized by X-ray powder diffraction (XRD) and transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS), and resonance Raman spectra.

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Metadata

Authors
Li, X.-L., & Li, Y.-D.
Venue
The Journal of Physical Chemistry B
Published
2004-08-21
Volume
108
Issue
37
Pages
13893-13900
ISSN
  • 1520-5207 (ISSN-L)
  • 1520-6106
OpenAlex
W2952735014
Cited by
233
References
1
FWCI
4.37
Type
journal article
Language
en
Open access
closed

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