The DOI matches its Crossref record; 58 of the 58 references it cites were found in a registry or an index.
Hydrothermal Synthesis of Single-Crystalline Anatase TiO2 Nanorods with Nanotubes as the Precursor
Abstract
Preparation of anatase TiO2 nanorods from solutions in the absence of surfactants or templates has rarely been reported. The present work has found that hydrothermal treatment of titanate nanotube suspensions under an acidic environment resulted in the formation of single-crystalline anatase nanorods with a specific crystal-elongation direction. The nanotube suspensions were prepared by treatment of TiO2 in NaOH, followed by mixing with HNO3 to different pH values. The crystal size of the anatase nanoparticles obtained from the hydrothermal treatment increased with the pH of the suspensions, and nanorods with an aspect ratio up to 6 and a long axis along the anatase [001] were obtained at a pH slightly less than 7. A mechanism for the tube-to-rod transformation has been proposed on the basis of the crystalline structures of the tubes and rods. The local shrinkage of the tube walls to form anatase crystallites and the subsequent oriented attachment of the crystallites have been suggested to be the key steps involved in the nanorod formation.
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Cites
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Cited by
TiO2 photocatalysis: Design and applications
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Protonated Titanates and TiO2 Nanostructured Materials: Synthesis, Properties, and Applications
Bavykin, D. V., Friedrich, J. M., & Walsh, F. C. (2006) · Advanced Materials · doi:10.1002/adma.200502696 · Cited by 1,634
Metadata
- Authors
- Nian, J.-N., & Teng, H.
- Venue
- The Journal of Physical Chemistry B
- Publisher
- American Chemical Society (ACS)
- Published
- 2006-02-14
- Volume
- 110
- Issue
- 9
- Pages
- 4193-4198
- ISSN
- 1520-5207 (ISSN-L)
- 1520-6106
- OpenAlex
- W2000754623
- Cited by
- 332
- References
- 58
- FWCI
- 19.44
- Type
- journal article
- Language
- en
- Open access
- closed
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
