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CeO2 Spherical Crystallites: Synthesis, Formation Mechanism, Size Control, and Electrochemical Property Study
Abstract
CeO 2 spherical crystallites aggregated by small CeO 2 nanoparticles in the diameter range of 5−10 nm were successfully fabricated through a facile surfactant-assisted hydrothermal method. PVP (poly(vinylpyrrolidone)) was applied as surfactant to facilitate the oriented aggregation of small CeO 2 nanoparticles into spherical crystallites. The size of as-obtained CeO 2 spherical crystallites could be deliberately controlled in the range 100−800 nm by varying synthetic parameters such as the molar ratio of PVP (repeating units) to Ce(NO 3 ) 3 ·6H 2 O and the concentration of Ce(NO 3 ) 3 ·6H 2 O solution. The formation mechanism was briefly discussed and the electrochemical properties of as-synthesized CeO 2 spherical crystallites were studied by galvanostatic methods. The electrochemical test results show that the as-obtained CeO 2 spherical crystallites have promising electrochemical properties that may enable them to be applied as an anode material in lithium ion batteries.
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Citations
Cited by
Fundamentals and Catalytic Applications of CeO 2 -Based Materials
Montini, T., Melchionna, M., Monai, M., & Fornasiero, P. (2016) · Chemical Reviews · doi:10.1021/acs.chemrev.5b00603 · Cited by 2,766
Liu, B., Li, C., Zhang, G., Yao, X., Chuang, S. S. C., & Li, Z. (2018) · ACS Catalysis · doi:10.1021/acscatal.8b00415 · Cited by 668
Metadata
- Authors
- Zhou, F., Zhao, X., Xu, H., & Yuan, C.
- Venue
- The Journal of Physical Chemistry C
- Publisher
- American Chemical Society (ACS)
- Published
- 2007-01-09
- Volume
- 111
- Issue
- 4
- Pages
- 1651-1657
- ISSN
- 1932-7447 (ISSN-L)
- 1932-7455
- OpenAlex
- W2003414003
- Cited by
- 192
- References
- 0
- FWCI
- 11.03
- Type
- journal article
- Language
- en
- Open access
- closed
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