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Hydrothermal Dehydration of Aqueous Fructose Solutions in a Closed System
Abstract
Aqueous monosaccharide solutions including glucose or fructose have been hydrothermally treated in a closed system to form colloidal carbon spheres. In-situ Raman and 13 C NMR have been used to quantify the intramolecular dehydration moiety, HMF, as an intermediate. An aqueous glucose solution forms a carbon sphere via an intermolecular dehydration route without forming HMF during initial hydrothermal treatment and followed by carbonization at 170−180 °C. However, an aqueous fructose solution initially forms HMF by intramolecular dehydration at 120−140 °C. Upon subsequent polymerization, microscopic carbon-containing spheres assemble to larger spheres, thereby generating a grain-like surface morphology. The carbon sphere contains a dense hydrophobic carbon core and a hydrophilic shell.
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Citations
Cited by
The production of carbon materials by hydrothermal carbonization of cellulose
Sevilla, M., & Fuertes, A. B. (2009) · Carbon · doi:10.1016/j.carbon.2009.04.026 · Cited by 2,021
Engineering carbon materials from the hydrothermal carbonization process of biomass
Hu, B., Wang, K., Wu, L., Yu, S., Antonietti, M., & Titirici, M. (2010) · Advanced Materials · doi:10.1002/adma.200902812 · Cited by 1,765
Libra, J. A., Ro, K. S., Kammann, C., Funke, A., Berge, N. D., Neubauer, Y., Titirici, M.-M., Fühner, C., Bens, O., Kern, J., et al. (2011) · Biofuels · doi:10.4155/bfs.10.81 · Cited by 1,756
Zhou, Y., Bao, Q., Tang, L. A. L., Zhong, Y., & Loh, K. P. (2009) · Chemistry of Materials · doi:10.1021/cm9006603 · Cited by 1,542
van Zandvoort, I., Wang, Y., Rasrendra, C. B., van Eck, E. R. H., Bruijnincx, P. C. A., Heeres, H. J., & Weckhuysen, B. M. (2013) · ChemSusChem · doi:10.1002/cssc.201300332 · Cited by 624
Metadata
- Authors
- Yao, C., Shin, Y., Wang, L.-Q., Windisch, Samuels, W. D., Arey, B. W., Wang, C., Risen, & Exarhos, G. J.
- Venue
- The Journal of Physical Chemistry C
- Publisher
- American Chemical Society (ACS)
- Published
- 2007-10-01
- Volume
- 111
- Issue
- 42
- Pages
- 15141-15145
- ISSN
- 1932-7447 (ISSN-L)
- 1932-7455
- OpenAlex
- W2036633413
- Cited by
- 303
- References
- 0
- FWCI
- 7.77
- Type
- journal article
- Language
- en
- Open access
- closed
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- Yao, C., Shin, Y., Wang, L.-Q., Windisch, Samuels, W. D., Arey, B. W., Wang, C., Risen, & Exarhos, G. J. (2007). Hydrothermal Dehydration of Aqueous Fructose Solutions in a Closed System. The Journal of Physical Chemistry C. https://doi.org/10.1021/jp074188l
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