Gas Permeation and Diffusion Characteristics of MFI-Type Zeolite Membranes at High Temperatures

Kanezashi, M.; Lin, Y. S.

doi:10.1021/jp804586q

Cited by 117Membrane Separation and Gas TransportZeolite Catalysis and SynthesisMetal-Organic Frameworks: Synthesis and Applications

The DOI matches its Crossref record; 34 of the 34 references it cites were found in a registry or an index.

Gas Permeation and Diffusion Characteristics of MFI-Type Zeolite Membranes at High Temperatures

Kanezashi, M., Lin, Y. S.·2009·The Journal of Physical Chemistry C

DOI 10.1021/jp804586q

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Abstract

MFI-type zeolite membranes were prepared by the template-free secondary growth method followed by onstream counter-diffusion or one-side chemical vapor deposition (CVD) modification to eliminate intercrystalline pores. Gas permeation and separation experiments were conducted on unmodified and modified membranes at 25−500 °C. For unmodified MFI-type zeolite membranes, single-gas permeation of H 2, He, CO, and CO 2 exhibits characteristics of Knudsen diffusion up to 500 °C, and adsorption of CO 2 on MFI-type zeolite has a strong effect on ternary gas separation (H 2, CO, and CO 2 ) below 300 °C. Counter-diffusion CVD modification is effective in sealing the intercrystalline gaps resulting in defect-free MFI-type zeolite membranes. Permeation of nonadsorbing gases (He, H 2, and CO) through counter-diffusion CVD-modified zeolite membranes also exhibits Knudsen diffusion characteristics with very small activation energies for diffusion (0.1−3 kJ mol −1 ), with gas permeance (diffusivity) decreasing with increasing molecular weight. For one-side CVD-modified MFI-type zeolite membranes, gas permeance (diffusivity) decreases and activation energy for diffusion increases with increasing molecular size because of the formation of an amorphous microporous silica layer. High-temperature gas permeation data on defect-free MFI-type zeolite membranes confirm the translational gas diffusion model for zeolites.

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Separation of H2 and CO has been studied on zeolitic MFI-type membranes.
“The separation of H2 and CO has been studied, as well, on zeolitic MFI-type membranes.563,564”
From Zeolites in Adsorption Processes: State of the Art and Future Prospects (2022) · cites this paper as [563]

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Authors: Kanezashi, M., & Lin, Y. S.
Affiliations: Hiroshima University (JP)
Corresponding author: Lin, Y. S.
ORCID: Kanezashi, M.
Lin, Y. S.
Venue: The Journal of Physical Chemistry C
Publisher: American Chemical Society (ACS)
Published: 2009-02-05
Volume: 113
Issue: 9
Pages: 3767-3774
ISSN: 1932-7447 (ISSN-L)
1932-7455
DOI: 10.1021/jp804586q
OpenAlex: W2013474579
Cited by: 115
References: 34
Citations by year: 2026: 5 · 2025: 5 · 2024: 7 · 2023: 4 · 2022: 5 · 2020: 5 · 2019: 5 · 2018: 6 · 2017: 12 · 2016: 6 · 2015: 9 · 2014: 6 · 2013: 11 · 2012: 8
FWCI: 19.37
Type: journal article
Language: en
Open access: closed
Locations: The Journal of Physical Chemistry C (publishedVersion)
Topics: Physical Sciences › Chemical Engineering › Filtration and Separation › Membrane Separation and Gas Transport
Physical Sciences › Chemistry › Inorganic Chemistry › Zeolite Catalysis and Synthesis
Physical Sciences › Chemistry › Inorganic Chemistry › Metal-Organic Frameworks: Synthesis and Applications
Keywords: gas permeation, gas separation, Knudsen diffusion, CO2 adsorption, hydrogen separation, CO2 separation, amorphous silica layer, diffusion activation energy, molecular weight dependence, zeolite membranes

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Gas Permeation and Diffusion Characteristics of MFI-Type Zeolite Membranes at High Temperatures

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