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Large Scale CVD Synthesis of Single-Walled Carbon Nanotubes
Abstract
The synthesis of bulk amounts of high quality single-walled carbon nanotubes (SWNTs) is accomplished by optimizing the chemical compositions and textural properties of the catalyst material used in the chemical vapor deposition (CVD) of methane. A series of catalysts are derived by systematically varying the catalytic metal compounds and support materials. The optimized catalysts consist of Fe/Mo bimetallic species supported on a novel silica−alumina multicomponent material. The high SWNT yielding catalyst exhibits high surface-area and large mesopore volume at elevated temperatures. Gram quantities of SWNT materials have been synthesized in ∼0.5 h using the optimized catalyst material. The nanotube material consists of individual and bundled SWNTs that are free of defects and amorphous carbon coating. This work represents a step forward toward obtaining kilogram scale perfect SWNT materials via simple CVD routes.
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Cites
Adsorption of Gases in Multimolecular Layers
Brunauer, S., Emmett, P. H., & Teller, E. (1938) · Journal of the American Chemical Society · doi:10.1021/ja01269a023 · Cited by 28,156
Cited by
Specific surface area of carbon nanotubes and bundles of carbon nanotubes
Peigney, A., Laurent, C., Flahaut, E., Bacsa, R. R., & Rousset, A. (2001) · Carbon · doi:10.1016/s0008-6223(00)00155-x · Cited by 2,040
Donaldson, K., Aitken, R., Tran, L., Stone, V., Duffin, R., Forrest, G., & Alexander, A. (2006) · Toxicological Sciences · doi:10.1093/toxsci/kfj130 · Cited by 1,167
Carbon nanotube applications for tissue engineering
Harrison, B. S., & Atala, A. (2007) · Biomaterials · doi:10.1016/j.biomaterials.2006.07.044 · Cited by 1,068
Direct Observation of Vapor−Liquid−Solid Nanowire Growth
Wu, Y., & Yang, P. (2001) · Journal of the American Chemical Society · doi:10.1021/ja0059084 · Cited by 1,040
Rathinavel, S., Priyadharshini, K., & Panda, D. (2021) · Materials Science and Engineering: B · doi:10.1016/j.mseb.2021.115095 · Cited by 845
Metadata
- Authors
- Cassell, A. M., Raymakers, J. A., Kong, J., & Dai, H.
- Venue
- The Journal of Physical Chemistry B
- Publisher
- American Chemical Society (ACS)
- Published
- 1999-07-20
- Volume
- 103
- Issue
- 31
- Pages
- 6484-6492
- ISSN
- 1520-5207 (ISSN-L)
- 1520-6106
- OpenAlex
- W1985588689
- Cited by
- 918
- References
- 1
- FWCI
- 22.59
- Type
- journal article
- Language
- en
- Open access
- closed
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- Cassell, A. M., Raymakers, J. A., Kong, J., & Dai, H. (1999). Large Scale CVD Synthesis of Single-Walled Carbon Nanotubes. The Journal of Physical Chemistry B. https://doi.org/10.1021/jp990957s
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
