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Synthesis and Self-Assembly of Amphiphilic Polymeric Microparticles
Abstract
We report the synthesis and self-assembly of amphiphilic, nonspherical, polymeric microparticles. Wedge-shaped particles bearing segregated hydrophilic and hydrophobic sections were synthesized in a microfludic channel by polymerizing across laminar coflowing streams of hydrophilic and hydrophobic polymers using continuous flow lithography (CFL). Particle monodispersity was characterized by measuring both the size of the particles formed and the extent of amphiphilicity. The coefficient of variation (COV) was found to be less than 2.5% in all measured dimensions. Particle structure was further characterized by measuring the curvature of the interface between the sections and the extent of cross-linking using FTIR spectroscopy. The amphiphilic particles were allowed to self-assemble in water or at water-oil interfaces. In water, the geometry of the particles enabled the formation of micelle-like structures, while in emulsions, the particles migrated to the oil-water interface and oriented themselves to minimize their surface energy.
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Cites
Permo-Triassic Boundary Superanoxia and Stratified Superocean: Records from Lost Deep Sea
Isozaki, Y. (1997) · Science · doi:10.1126/science.276.5310.235 · Cited by 842
Cited by
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Walther, A., & Müller, A. H. E. (2013) · Chemical Reviews · doi:10.1021/cr300089t · Cited by 1,769
Janus Particle Synthesis and Assembly
Jiang, S., Chen, Q., Tripathy, M., Luijten, E., Schweizer, K. S., & Granick, S. (2010) · Advanced Materials · doi:10.1002/adma.200904094 · Cited by 803
Synthesis of micro and nanostructures in microfluidic systems
Marre, S., & Jensen, K. F. (2010) · Chemical Society Reviews · doi:10.1039/b821324k · Cited by 734
pH-sensitive poly (histidine)-PEG/DSPE-PEG co-polymer micelles for cytosolic drug delivery
Wu, H., Zhu, L., & Torchilin, V. P. (2013) · Biomaterials · doi:10.1016/j.biomaterials.2012.08.072 · Cited by 355
Metadata
- Authors
- Dendukuri, D., Hatton, T. A., & Doyle, P. S.
- Venue
- Langmuir
- Publisher
- American Chemical Society (ACS)
- Published
- 2006-12-08
- Volume
- 23
- Issue
- 8
- Pages
- 4669-4674
- ISSN
- 0743-7463 (ISSN-L)
- 1520-5827
- OpenAlex
- W2008049034
- Cited by
- 162
- References
- 1
- FWCI
- 8.03
- Type
- journal article
- Language
- en
- Open access
- closed
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