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Electrochemical and Spectroscopic Analysis of Mg2+ Intercalation into Thin Film Electrodes of Layered Oxides: V2O5 and MoO3
Abstract
Electrochemical, surface, and structural studies related to rechargeable Mg batteries were carried out with monolithic thin-film cathodes comprising layered V2O5 and MoO3. The reversible intercalation reactions of these electrodes with Mg ion in nonaqueous Mg salt solutions were explored using a variety of analytical tools. These included slow-scan rate cyclic voltammetry (SSCV), chrono-potentiometry (galvanostatic cycling), Raman and photoelectron spectroscopies, high-resolution microscopy, and XRD. The V2O5 electrodes exhibited reversible Mg-ion intercalation at capacities around 150-180 mAh g(-1) with 100% efficiency. A capacity of 220 mAh g(-1) at >95% efficiency was obtained with MoO3 electrodes. By applying the electrochemical driving force sufficiently slowly it was possible to measure the electrodes at equilibrium conditions and verify by spectroscopy, microscopy, and diffractometry that these electrodes undergo fully reversible structural changes upon Mg-ion insertion/deinsertion cycling.
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Citations
Cited by
Quest for Nonaqueous Multivalent Secondary Batteries: Magnesium and Beyond
Muldoon, J., Bucur, C. B., & Gregory, T. (2014) · Chemical Reviews · doi:10.1021/cr500049y · Cited by 1,376
Nanostructured Mo-based electrode materials for electrochemical energy storage
Hu, X., Zhang, W., Liu, X., Mei, Y., & Huang, Y. (2015) · Chemical Society Reviews · doi:10.1039/c4cs00350k · Cited by 711
Materials Design Rules for Multivalent Ion Mobility in Intercalation Structures
Rong, Z., Malik, R., Canepa, P., Sai Gautam, G., Liu, M., Jain, A., Persson, K., & Ceder, G. (2015) · Chemistry of Materials · doi:10.1021/acs.chemmater.5b02342 · Cited by 561
Vanadium‐Based Nanomaterials: A Promising Family for Emerging Metal‐Ion Batteries
Xu, X., Xiong, F., Meng, J., Wang, X., Niu, C., An, Q., & Mai, L. (2020) · Advanced Functional Materials · doi:10.1002/adfm.201904398 · Cited by 482
Micro‐ and Nano‐Structured Vanadium Pentoxide (V2O5) for Electrodes of Lithium‐Ion Batteries
Yue, Y., & Liang, H. (2017) · Advanced Energy Materials · doi:10.1002/aenm.201602545 · Cited by 382
Metadata
- Authors
- Gershinsky, G., Yoo, H. D., Gofer, Y., & Aurbach, D.
- Venue
- Langmuir
- Publisher
- American Chemical Society (ACS)
- Published
- 2013-08-07
- Volume
- 29
- Issue
- 34
- Pages
- 10964-10972
- ISSN
- 0743-7463 (ISSN-L)
- 1520-5827
- OpenAlex
- W1964907830
- Cited by
- 385
- References
- 0
- FWCI
- 15.18
- Type
- journal article
- Language
- en
- Open access
- closed
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- Gershinsky, G., Yoo, H. D., Gofer, Y., & Aurbach, D. (2013). Electrochemical and Spectroscopic Analysis of Mg2+ Intercalation into Thin Film Electrodes of Layered Oxides: V2O5 and MoO3. Langmuir. https://doi.org/10.1021/la402391f
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