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Rheology of End-Tethered Polymer Layered Silicate Nanocomposites
Abstract
The rheology of end-tethered polymer layered silicate nanocomposites is investigated using linear viscoelastic measurements in oscillatory shear with small strain amplitudes. Two systems consisting of poly(ε-caprolactone) and nylon-6 with varying amounts of layered silicate (montmorillonite) are examined. The storage ( G ‘) and loss ( G ‘‘) moduli increase at all frequencies with increasing silicate loading, consistent with previous findings with conventionally filled polymer systems. However, the power-law dependence of G ‘ and G ‘‘ in the terminal zone is different from that observed in homopolymers and decreases with increasing silicate loading. At low frequencies the rheological response becomes almost invariant with frequency, suggestive of a solid-like response. Comparisons are drawn with rheology of other intrinsically anisotropic materials, and an attempt is made to explain phenomenologically their rich-rheological behavior.
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Cites
Stress relaxation in the lamellar copolymer mesophase
Witten, T. A., Leibler, L., & Pincus, P. A. (1990) · Macromolecules · doi:10.1021/ma00205a022 · Cited by 202
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Moniruzzaman, M., & Winey, K. I. (2006) · Macromolecules · doi:10.1021/ma060733p · Cited by 3,416
Graphene/Polymer Nanocomposites
Kim, H., Abdala, A. A., & Macosko, C. W. (2010) · Macromolecules · doi:10.1021/ma100572e · Cited by 3,406
SINHARAY, S., & BOUSMINA, M. (2005) · Progress in Materials Science · doi:10.1016/j.pmatsci.2005.05.002 · Cited by 1,611
Nano-biocomposites: Biodegradable polyester/nanoclay systems
BORDES, P., POLLET, E., & AVEROUS, L. (2009) · Progress in Polymer Science · doi:10.1016/j.progpolymsci.2008.10.002 · Cited by 1,033
New polylactide/layered silicate nanocomposites. 1. Preparation, characterization, and properties
Sinha Ray, S., Maiti, P., Okamoto, M., Yamada, K., & Ueda, K. (2002) · Macromolecules · doi:10.1021/ma011613e · Cited by 607
Metadata
- Authors
- Krishnamoorti, R., & Giannelis, E. P.
- Venue
- Macromolecules
- Publisher
- American Chemical Society (ACS)
- Published
- 1997-07-01
- Volume
- 30
- Issue
- 14
- Pages
- 4097-4102
- ISSN
- 0024-9297 (ISSN-L)
- 1520-5835
- OpenAlex
- W2062829152
- Cited by
- 779
- References
- 1
- FWCI
- 5.34
- Type
- journal article
- Language
- en
- Open access
- closed
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Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
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