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Radial Anisotropic Growth of Rhodium Nanoparticles
Abstract
In this contribution, we report the synthesis of rhodium multipods that result from a homogeneous seeded growth mechanism. Small Rh nanocrystal seeds were synthesized by the reduction of RhCl3 in ethylene glycol in the presence of PVP. These seed particles could be subsequently used, without isolation, to form larger rhodium nanoparticles. A reaction temperature of 190 degrees C led to isotropic cubic Rh particles. Lowering the reaction temperature resulted in more anisotropic growth, which gave Rh cubes with horns at 140 degrees C, and Rh multipods at 90 degrees C. The anisotropic growth occurred in the (111) direction, as determined by high-resolution TEM (HRTEM). Anisotropic growth proceeds via a seeded growth mechanism, and not by oriented attachment.
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Cited by
Shape‐Controlled Synthesis of Metal Nanocrystals: Simple Chemistry Meets Complex Physics?
Xia, Y., Xiong, Y., Lim, B., & Skrabalak, S. E. (2009) · Angewandte Chemie International Edition · doi:10.1002/anie.200802248 · Cited by 5,702
Shape Control of Colloidal Metal Nanocrystals
Tao, A. R., Habas, S., & Yang, P. (2008) · Small · doi:10.1002/smll.200701295 · Cited by 2,408
Synthesis of Platinum Multipods: An Induced Anisotropic Growth
Teng, X., & Yang, H. (2005) · Nano Letters · doi:10.1021/nl0503072 · Cited by 279
Facile Aqueous‐Phase Synthesis of Uniform Palladium Nanoparticles of Various Shapes and Sizes
Piao, Y., Jang, Y., Shokouhimehr, M., Lee, I. S., & Hyeon, T. (2007) · Small · doi:10.1002/smll.200600402 · Cited by 173
Shape-controlled syntheses of rhodium nanocrystals for the enhancement of their catalytic properties
Xie, S., Liu, X. Y., & Xia, Y. (2015) · Nano Research · doi:10.1007/s12274-014-0674-x · Cited by 104
Metadata
- Authors
- Hoefelmeyer, J. D., Niesz, K., Somorjai, G. A., & Tilley, T. D.
- Venue
- Nano Letters
- Publisher
- American Chemical Society (ACS)
- Published
- 2005-02-01
- Volume
- 5
- Issue
- 3
- Pages
- 435-438
- ISSN
- 1530-6984 (ISSN-L)
- 1530-6992
- OpenAlex
- W2002079581
- Cited by
- 208
- References
- 0
- FWCI
- 12.06
- Type
- journal article
- Language
- en
- Open access
- closed
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- Hoefelmeyer, J. D., Niesz, K., Somorjai, G. A., & Tilley, T. D. (2005). Radial Anisotropic Growth of Rhodium Nanoparticles. Nano Letters. https://doi.org/10.1021/nl048100g
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