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Synthesis of Platinum Nanowire Networks Using a Soft Template
Open accessAbstract
Platinum nanowire networks have been synthesized by chemical reduction of a platinum complex using sodium borohydride in the presence of a soft template formed by cetyltrimethylammonium bromide in a two-phase water-chloroform system. The interconnected polycrystalline nanowires possess the highest surface area (53 +/- 1 m2/g) and electroactive surface area (32.4 +/- 3.6 m2/g) reported for unsupported platinum nanomaterials; the high surface area results from the small average diameter of the nanowires (2.2 nm) and the 2-10 nm pores determined by nitrogen adsorption measurements. Synthetic control over the network was achieved simply by varying the stirring rate and reagent concentrations, in some cases leading to other types of nanostructures including wormlike platinum nanoparticles. Similarly, substitution of a palladium complex for platinum gives palladium nanowire networks. A mechanism of formation of the metal nanowire networks is proposed based on confined metal growth within a soft template consisting of a network of swollen inverse wormlike micelles.
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Cites
Catalytic nanoarchitectures—The importance of nothing and the unimportance of periodicity
Rolison, D. R. (2003) · Science · doi:10.1126/science.1082332 · Cited by 1,037
Formation of carbon-supported PtM alloys for low temperature fuel cells: a review
Antolini, E. (2003) · Materials Chemistry and Physics · doi:10.1016/s0254-0584(02)00389-9 · Cited by 624
Cited by
Shape‐Controlled Synthesis of Metal Nanocrystals: Simple Chemistry Meets Complex Physics?
Xia, Y., Xiong, Y., Lim, B., & Skrabalak, S. E. (2009) · Angewandte Chemie International Edition · doi:10.1002/anie.200802248 · Cited by 5,702
Platinum-Based Nanostructured Materials: Synthesis, Properties, and Applications
Chen, A., & Holt-Hindle, P. (2010) · Chemical Reviews · doi:10.1021/cr9003902 · Cited by 1,390
Peng, Z., & Yang, H. (2009) · Nano Today · doi:10.1016/j.nantod.2008.10.010 · Cited by 1,085
Shape-controlled synthesis of platinum nanocrystals for catalytic and electrocatalytic applications
Chen, J., Lim, B., Lee, E. P., & Xia, Y. (2009) · Nano Today · doi:10.1016/j.nantod.2008.09.002 · Cited by 852
Zhu, C., Du, D., Eychmüller, A., & Lin, Y. (2015) · Chemical Reviews · doi:10.1021/acs.chemrev.5b00255 · Cited by 672
Metadata
- Authors
- Song, Y., Garcia, R. M., Dorin, R. M., Wang, H., Qiu, Y., Coker, E. N., Steen, W. A., Miller, J. E., & Shelnutt, J. A.
- Venue
- Nano Letters
- Publisher
- American Chemical Society (ACS)
- Published
- 2007-11-14
- Volume
- 7
- Issue
- 12
- Pages
- 3650-3655
- ISSN
- 1530-6984 (ISSN-L)
- 1530-6992
- OpenAlex
- W1982689642
- Cited by
- 343
- References
- 2
- FWCI
- 14.67
- Type
- journal article
- Language
- en
- Open access
- green
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- Song, Y., Garcia, R. M., Dorin, R. M., Wang, H., Qiu, Y., Coker, E. N., Steen, W. A., Miller, J. E., & Shelnutt, J. A. (2007). Synthesis of Platinum Nanowire Networks Using a Soft Template. Nano Letters. https://doi.org/10.1021/nl0719123
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