The DOI matches its Crossref record; 1 of the 1 references it cites were found in a registry or an index.
In Situ Transmission Electron Microscopy of Lead Dendrites and Lead Ions in Aqueous Solution
Open accessAbstract
An ideal technique for observing nanoscale assembly would provide atomic-resolution images of both the products and the reactants in real time. Using a transmission electron microscope we image in situ the electrochemical deposition of lead from an aqueous solution of lead(II) nitrate. Both the lead deposits and the local Pb(2+) concentration can be visualized. Depending on the rate of potential change and the potential history, lead deposits on the cathode in a structurally compact layer or in dendrites. In both cases the deposits can be removed and the process repeated. Asperities that persist through many plating and stripping cycles consistently nucleate larger dendrites. Quantitative digital image analysis reveals excellent correlation between changes in the Pb(2+) concentration, the rate of lead deposition, and the current passed by the electrochemical cell. Real-time electron microscopy of dendritic growth dynamics and the associated local ionic concentrations can provide new insight into the functional electrochemistry of batteries and related energy storage technologies.
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Cites
Solvent Structure, Dynamics, and Ion Mobility in Aqueous Solutions at 25 °C
Koneshan, S., Rasaiah, J. C., Lynden-Bell, R. M., & Lee, S. H. (1998) · The Journal of Physical Chemistry B · doi:10.1021/jp980642x · Cited by 965
Cited by
Design principles for electrolytes and interfaces for stable lithium-metal batteries
Tikekar, M. D., Choudhury, S., Tu, Z., & Archer, L. A. (2016) · Nature Energy · doi:10.1038/nenergy.2016.114 · Cited by 1,765
Electron–Water Interactions and Implications for Liquid Cell Electron Microscopy
Schneider, N. M., Norton, M. M., Mendel, B. J., Grogan, J. M., Ross, F. M., & Bau, H. H. (2014) · The Journal of Physical Chemistry C · doi:10.1021/jp507400n · Cited by 654
A Review of Solid Electrolyte Interphase (SEI) and Dendrite Formation in Lithium Batteries
Li, B., Chao, Y., Li, M., Xiao, Y., Li, R., Yang, K., Cui, X., Xu, G., Li, L., Yang, C., et al. (2023) · Electrochemical Energy Reviews · doi:10.1007/s41918-022-00147-5 · Cited by 406
Zeng, Z., Liang, W.-I., Liao, H.-G., Xin, H. L., Chu, Y.-H., & Zheng, H. (2014) · Nano Letters · doi:10.1021/nl403922u · Cited by 379
Bubble and Pattern Formation in Liquid Induced by an Electron Beam
Grogan, J. M., Schneider, N. M., Ross, F. M., & Bau, H. H. (2014) · Nano Letters · doi:10.1021/nl404169a · Cited by 346
Metadata
- Authors
- White, E. R., Singer, S. B., Augustyn, V., Hubbard, W. A., Mecklenburg, M., Dunn, B., & Regan, B. C.
- Venue
- ACS Nano
- Publisher
- American Chemical Society (ACS)
- Published
- 2012-06-28
- Volume
- 6
- Issue
- 7
- Pages
- 6308-6317
- ISSN
- 1936-0851 (ISSN-L)
- 1936-086X
- OpenAlex
- W2021481086
- Cited by
- 187
- References
- 1
- FWCI
- 10.58
- Type
- journal article
- Language
- en
- Open access
- green
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